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[ CAS No. 37676-90-7 ] {[proInfo.proName]}

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Chemical Structure| 37676-90-7
Chemical Structure| 37676-90-7
Structure of 37676-90-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 37676-90-7 ]

CAS No. :37676-90-7 MDL No. :MFCD18806719
Formula : C7H10O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 126.15 Pubchem ID :-
Synonyms :

Safety of [ 37676-90-7 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 37676-90-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 37676-90-7 ]

[ 37676-90-7 ] Synthesis Path-Downstream   1~25

  • 1
  • [ 37676-90-7 ]
  • [ 37676-95-2 ]
YieldReaction ConditionsOperation in experiment
With tetrachloromethane; bromine
  • 2
  • [ 408314-33-0 ]
  • [ 37676-90-7 ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; toluene
  • 3
  • [ 408314-33-0 ]
  • [ 37676-90-7 ]
  • 1-hydroxy-3,3-dimethyl-cyclobutanecarboxylic acid methyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; toluene Behandeln des Reaktionsprodukts mit Diazomethan in Aether;
  • 4
  • [ 19251-73-1 ]
  • [ 37676-90-7 ]
YieldReaction ConditionsOperation in experiment
(i) TsOMe, (ii) aq. KOH; Multistep reaction;
  • 5
  • [ 64-17-5 ]
  • [ 37676-90-7 ]
  • [ 37676-92-9 ]
  • 6
  • [ 37676-90-7 ]
  • [ 503-53-7 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride
  • 7
  • [ 37676-90-7 ]
  • [ 75017-17-3 ]
YieldReaction ConditionsOperation in experiment
With lithium aluminium tetrahydride; hydrogen Multistep reaction;
  • 8
  • [ 20104-44-3 ]
  • [ 37676-90-7 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; methyl iodide 1.) 80 deg C, 4 h, 2.) 80 deg C, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
  • 9
  • [ 20104-44-3 ]
  • [ 37676-90-7 ]
  • [ 75017-16-2 ]
YieldReaction ConditionsOperation in experiment
Yield given. Multistep reaction. Yields of byproduct given;
YieldReaction ConditionsOperation in experiment
Rk. m. sd. wss. HCl (15 Stdn.) -> 4-Carboxy-2.2-dimethyl-butanal;
YieldReaction ConditionsOperation in experiment
Beh. v. 1-Methoxycarbonyl-2-trimethylamino-3.3-dimethyl-cyclobutantosylat m. wss. KOH Lsg.;
(yield)81percent;
  • 12
  • [ 37676-90-7 ]
  • [ 76207-24-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1.) H2, 2.) LiAlH4 2: pyridine / 0 °C
  • 13
  • [ 37676-90-7 ]
  • [ 75017-23-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 1.) H2, 2.) LiAlH4 2: pyridine / 0 °C 3: LiCl / hexamethylphosphoric acid triamide / Ambient temperature
  • 14
  • [ 37676-90-7 ]
  • [ 71385-29-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 4: aq. HCl
  • 16
  • [ 37676-90-7 ]
  • 3,3-Dimethyl-2-(propylamino)-cyclobutancarbonsaeure-aethylester [ No CAS ]
  • 17
  • [ 37676-90-7 ]
  • [ 92329-72-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 2: (i), (ii) /BRN= 605303/, Py
  • 18
  • tert-butyl 2-(N-pyrrolidino)-3,3-dimethylcyclobutane-1-carboxylate [ No CAS ]
  • [ 37676-90-7 ]
  • [ 1373621-73-8 ]
YieldReaction ConditionsOperation in experiment
1: 69% 2: 6% Stage #1: tert-butyl 2-(N-pyrrolidino)-3,3-dimethylcyclobutane-1-carboxylate With methyl p-toluene sulfonate In acetonitrile at 20℃; Stage #2: With potassium hydroxide In water; acetonitrile Reflux; Stage #3: With hydrogenchloride In water; acetonitrile Cooling;
1: 49% 2: 45% Stage #1: tert-butyl 2-(N-pyrrolidino)-3,3-dimethylcyclobutane-1-carboxylate With methyl iodide In acetonitrile at 20℃; for 14h; Stage #2: With potassium <i>tert</i>-butylate In diethyl ether for 4h; Reflux; Stage #3: With hydrogenchloride In diethyl ether; water Cooling;
  • 19
  • [ 37676-90-7 ]
  • tert-butyl cis-2-[(S)-N-α-methylbenzyl-N-benzylamino]-3,3-dimethylcyclobutane-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: sulfuric acid / dichloromethane / -78 - -25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C 2.2: 20 °C / Cooling
  • 20
  • [ 37676-90-7 ]
  • tert-butyl trans-2-[(S)-N-α-methylbenzyl-N-benzylamino]-3,3-dimethylcyclobutane-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: sulfuric acid / dichloromethane / -78 - -25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C 2.2: 20 °C / Cooling
  • 21
  • [ 37676-90-7 ]
  • trans-2-amino-3,3-dimethylcyclobutane-1-carboxylic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: sulfuric acid / dichloromethane / -78 - -25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C 2.2: 20 °C / Cooling 3.1: 20 % Pd(OH)2/C; hydrogen; acetic acid / 20 h / 60 °C / 2280.15 Torr 3.2: 24 h / 20 °C 3.3: Dowex 50X8 20-50 mesh
  • 22
  • [ 37676-90-7 ]
  • tert-butyl-2-(N,N-dibenzylamino)-3,3-dimethylcyclobutane-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: sulfuric acid / dichloromethane / -78 - -25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 0 °C 2.2: 20 °C
  • 23
  • [ 37676-90-7 ]
  • tert-butyl (+/-)-cis-2-(N,N-dibenzylamino)-3,3-dimethylcyclobutane-1-carboxylate [ No CAS ]
  • tert-butyl (+/-)-trans-2-(N,N-dibenzylamino)-3,3-dimethylcyclobutane-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: sulfuric acid / dichloromethane / -78 - -25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 0 °C 2.2: 20 °C
  • 24
  • [ 37676-90-7 ]
  • tert-butyl (+/-)-trans-2-(N,N-dibenzylamino)-3,3-dimethylcyclobutane-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: sulfuric acid / dichloromethane / -78 - -25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 0 °C 2.2: 20 °C 3.1: sodium hexamethyldisilazane; <i>tert</i>-butyl alcohol / tetrahydrofuran / 120 h
  • 25
  • [ 37676-90-7 ]
  • [ 115-11-7 ]
  • [ 1373621-73-8 ]
YieldReaction ConditionsOperation in experiment
97% With sulfuric acid In dichloromethane at -78 - -25℃;
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