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[ CAS No. 38462-22-5 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 38462-22-5
Chemical Structure| 38462-22-5
Chemical Structure| 38462-22-5
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Product Details of [ 38462-22-5 ]

CAS No. :38462-22-5 MDL No. :MFCD00012393
Formula : C10H18OS Boiling Point : -
Linear Structure Formula :- InChI Key :RVOKNSFEAOYULQ-UHFFFAOYSA-N
M.W : 186.31 Pubchem ID :61982
Synonyms :

Safety of [ 38462-22-5 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P273-P301+P310-P305+P351+P338 UN#:2810
Hazard Statements:H301-H319-H400 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 38462-22-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 38462-22-5 ]

[ 38462-22-5 ] Synthesis Path-Downstream   1~15

  • 1
  • [ 38462-22-5 ]
  • [ 10458-14-7 ]
YieldReaction ConditionsOperation in experiment
95% With di-tert-butyl peroxide; triethyl phosphite In acetonitrile at 20℃; UV-irradiation; 15 Example 15 Use 0.75 mmol of substrate according to the general procedure.DTBP (1.2 equiv.),P(OEt)3 (2.0 equiv.),Reaction solvent CH3CN (6 ml).After the reaction,Evaporate the solvent under reduced pressure.Crude product through column (petroleum ether / ethyl acetate = 20:1)Separated 109.9 mg of a colorless liquid,It is the product, the yield is 95%.
95% With di-tert-butyl peroxide; triethyl phosphite In acetonitrile at 25℃; for 6h; Irradiation;
78% With triethyl borane; tributylphosphine; triethyl phosphite In acetonitrile for 36h; Irradiation;
YieldReaction ConditionsOperation in experiment
Pulegon, H2S;
Examples of thiols R1XH or R2XH are: 3-mercapto-1-hexanol 2-(1-mercapto-1-methylethyl)-5-methylcyclohexanone methoxy-4-methyl-2-butane-2-thiol thiogeraniol thioterpineol.
13 Preparation of menthone-8-thiol EXAMPLE 13 Preparation of menthone-8-thiol The reaction was carried out as described in Example 7 using 10 g. of isopulegone (αD20 = 124.2°), 50 g. of H2 S and 0.1 g. of triethylamine. After fractionating, 69.4% of menthone-8-thiol, αD20 = - 12.0°, were obtained as a mixture of cis-trans compounds.
Pulegon, H2S;
..., H2S;

  • 3
  • [ 94293-57-9 ]
  • [ 38462-22-5 ]
YieldReaction ConditionsOperation in experiment
With Passiflora edulis wall-bound hydrolase at 30℃; aq. phosphate buffer; Enzymatic reaction;
  • 5
  • [ 38462-22-5 ]
  • C27H35N2O3PS [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: hydrogenchloride; sodium nitrite / methanol; water / 20 °C / Darkness 2: tetrahydrofuran / 20 °C / pH 7.4
  • 6
  • [ 38462-22-5 ]
  • C10H17NO2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; sodium nitrite In methanol; water at 20℃; Darkness; Preparation of S-nitrosothiols General procedure: The thiol starting material (RSH, 0.2 mmol) was dissolved in 1 ml of MeOHfollowed by the addition of 1 N HCl (1 ml) at room temperature. To thissolution was then added freshly prepared 1 N NaNO2 (1 ml) in water in dark(total c=0.07 M). The color of the reaction was immediately turned to red(for primary and secondary RSNO) or green (for tertiary RSNO). The mixturewas stirred for 10-15 min at room temperature. Upon completion (monitoredby TLC), the RSNO product was directly extracted with cold diethyl ether(1 ml× 3) in dark. The organic layers were collected and dried. The solvent wasremoved to provide the RSNO product that was then used for the ligationreaction without further purification.
  • 7
  • [ 38462-22-5 ]
  • cis-2-(2-(allylsulfonyl)propan-2-yl)-5-methylcyclohexan-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: potassium carbonate / methanol / Inert atmosphere; Reflux 2: sodium perborate tetrahydrate; acetic acid / 24 h
  • 8
  • [ 38462-22-5 ]
  • cis-5-methyl-2-(2-methyl-4-phenylbut-3-yn-2-yl)cyclohexan-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: potassium carbonate / methanol / Inert atmosphere; Reflux 2: sodium perborate tetrahydrate; acetic acid / 24 h 3: 2,2'-azobis(isobutyronitrile) / chloroform / 48 h / 85 °C / Inert atmosphere; Schlenk technique
  • 9
  • [ 38462-22-5 ]
  • cis-2-(2-azidopropan-2-yl)-5-methylcyclohexan-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: potassium carbonate / methanol / Inert atmosphere; Reflux 2: sodium perborate tetrahydrate; acetic acid / 24 h 3: dilauryl peroxide / chloroform / 48 h / 85 °C / Inert atmosphere; Schlenk technique
  • 10
  • [ 38462-22-5 ]
  • cis-5-methyl-2-(propan-2-yl-2-d)cyclohexan-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: potassium carbonate / methanol / Inert atmosphere; Reflux 2: sodium perborate tetrahydrate; acetic acid / 24 h 3: 2,2'-azobis(isobutyronitrile); water-d2 / chloroform / 24 h / 85 °C / Inert atmosphere; Schlenk technique
  • 11
  • [ 38462-22-5 ]
  • [ 106-95-6 ]
  • C13H22OS [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate In methanol Inert atmosphere; Reflux;
  • 12
  • dimethyl-4-nitrophenylsulfonium trifluoromethanesulfonate [ No CAS ]
  • [ 38462-22-5 ]
  • 5-methyl-2-(2-((4-nitrophenyl)thio)propan-2-yl)cyclohexan-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 3h; Inert atmosphere; Schlenk technique;
  • 13
  • [ 38462-22-5 ]
  • [ 7230-16-2 ]
YieldReaction ConditionsOperation in experiment
97% With di-tert-butyl peroxide; water-d2; ethydiphenylphosphine oxide at 20℃; for 6h; Sealed tube; Irradiation; 12; 13 The general operational flow of the experiment General procedure: The reaction substrate is added to a mixed solvent of dichloromethane and deuterated water (V: V = 2: 1), and Ph2POEt and DTBP are sequentially added; The mouth of the bottle was sealed with a stopper and stirring was started, and the reaction system was placed under the irradiation of two 36 W fluorescent lamps for 6 hours at room temperature. After completion of the reaction, the solvent was distilled off under reduced pressure, and the product was separated by chromatography
95% With di-tert-butyl peroxide; water-d2; ethydiphenylphosphine oxide In dichloromethane at 20℃; for 10h; Irradiation; Green chemistry;
  • 14
  • [ 530-48-3 ]
  • [ 38462-22-5 ]
  • 2-(2-((2,2-diphenylvinyl)thio)propan-2-yl)-5-methylcyclohexan-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
20% With dmap; cadmium selenide In acetonitrile at 20℃; for 12h; Irradiation; Sealed tube;
  • 15
  • [ 624-92-0 ]
  • [ 38462-22-5 ]
  • C11H20OS2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
91% With Na-exchanged X type zeolite catalyst In ethanol at 10℃; for 20h;
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