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[ CAS No. 42464-96-0 ] {[proInfo.proName]}

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Chemical Structure| 42464-96-0
Chemical Structure| 42464-96-0
Structure of 42464-96-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 42464-96-0 ]

CAS No. :42464-96-0 MDL No. :
Formula : C10H11IN2 Boiling Point : -
Linear Structure Formula :- InChI Key :JPEZFBFIRRAFNR-UHFFFAOYSA-N
M.W : 286.11 Pubchem ID :66522933
Synonyms :

Safety of [ 42464-96-0 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P312-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 42464-96-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 42464-96-0 ]

[ 42464-96-0 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 71636-07-2 ]
  • [ 42464-96-0 ]
YieldReaction ConditionsOperation in experiment
With iron; acetic acid
  • 2
  • [ 42464-96-0 ]
  • [ 861393-93-3 ]
YieldReaction ConditionsOperation in experiment
With hydrogen In acetic acid at 20℃; for 48h; 43A The iodide salt of 5-amino-1-methylquinolinium (3 g, 9.5 mmol), (prepared as described in McCurdy et al., J. Am. Chem. Soc. Vol. 114(26) pages 10314-21 (1992)), in 250 ml of acetic acid was treated with PtO2 (0.6 g) under hydrogen at 50 psi for 48 hr at room temperature. To the precipitated tan-colored product was added 100 ml of methanol to homogenize for filtration. Filtrate was concentrated, dissolved in methylene chloride, cooled, neutralized with 1M NaHCO3 to pH 7, and finally extracted with methylene chloride. The combined organic layers were dried (Na2SO4), filtered, and the filtrate was concentrated to provide the title compound. MS (ESI+) m/z 163 (M+H)+.
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