Home Cart 0 Sign in  
X

[ CAS No. 479544-59-7 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
3d Animation Molecule Structure of 479544-59-7
Chemical Structure| 479544-59-7
Chemical Structure| 479544-59-7
Structure of 479544-59-7 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 479544-59-7 ]

Related Doc. of [ 479544-59-7 ]

Alternatived Products of [ 479544-59-7 ]

Product Details of [ 479544-59-7 ]

CAS No. :479544-59-7 MDL No. :N/A
Formula : C12H18O4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 226.27 Pubchem ID :-
Synonyms :

Safety of [ 479544-59-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 479544-59-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 479544-59-7 ]

[ 479544-59-7 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 884539-90-6 ]
  • [ 479544-59-7 ]
  • C44H62N2O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
92% With dmap; dicyclohexyl-carbodiimide In dichloromethane for 12h; Reflux; Inert atmosphere;
  • 2
  • [ 479544-59-7 ]
  • C46H46N2O2S2 [ No CAS ]
  • C58H62N2O5S2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
67.8% With N,N-dimethyl-4-aminopyridine; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; Inert atmosphere; 2.2.5. Synthesis of monomer TP 4-(4-cycloocten-1-yloxy)-4-oxobutanoic acid was synthesized according to a literature [45]. Compound 4 (7.23 g, 10 mmol), 4-(4-cycloocten-1-yloxy)-4-oxobutanoic acid (2.71 g, 12 mmol) and 4-dimethylaminopyridine (DMAP) (1.22 g, 10 mmol) were soluble in 50 mL anhydrous dichloromethane. N, N-dicyclohexylcarbodiimide (DCC) solution (6.18 g, 30 mmol in 30 mL dichloromethane) was added into the mixture slowly at 0 °C under nitrogen atmosphere. Then the mixture was warmed up to room temperature and stirred for 24 h. After purifying by column chromatography (petroleum ether: chloroform = 1: 2), the target monomer TP was obtained in the yield of 67.8%. 1H NMR (400 MHz, Chloroform-d) δ 7.74 (d, J = 2.4 Hz, 1H), 7.56 (s, 1H), 7.53 (d, J =2.5 Hz, 1H), 7.45 (s, 0H), 7.26 (d, J = 3.1 Hz, 2H), 7.15 (s, 1H),7.12-7.09 (m, 2H), 7.01 (d, J = 8.7 Hz, 1H), 6.95 (d, J = 1.9 Hz, 1H),6.93 (s, 1H), 5.65 (s, 1H), 4.87 (s, 1H), 4.04-3.99 (m, 2H), 2.61 (s, 2H),2.12 (s, 2H), 1.86 (dd, J = 10.0, 5.8 Hz, 4H), 1.55 (s, 9H).
  • 3
  • [ 479544-59-7 ]
  • C28H48O2 [ No CAS ]
  • C40H64O5 [ No CAS ]
YieldReaction ConditionsOperation in experiment
67.3% With N,N-dimethyl-4-aminopyridine; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; Inert atmosphere; 2.2.5. Synthesis of monomer TP General procedure: 4-(4-cycloocten-1-yloxy)-4-oxobutanoic acid was synthesized according to a literature [45]. Compound 4 (7.23 g, 10 mmol), 4-(4-cycloocten-1-yloxy)-4-oxobutanoic acid (2.71 g, 12 mmol) and 4-dimethylaminopyridine (DMAP) (1.22 g, 10 mmol) were soluble in 50 mL anhydrous dichloromethane. N, N-dicyclohexylcarbodiimide (DCC) solution (6.18 g, 30 mmol in 30 mL dichloromethane) was added into the mixture slowly at 0 °C under nitrogen atmosphere. Then the mixture was warmed up to room temperature and stirred for 24 h. After purifying by column chromatography (petroleum ether: chloroform = 1: 2), the target monomer TP was obtained in the yield of 67.8%.
Same Skeleton Products
Historical Records