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Chemical Structure| 51075-37-7 Chemical Structure| 51075-37-7

Structure of 51075-37-7

Chemical Structure| 51075-37-7

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Product Details of [ 51075-37-7 ]

CAS No. :51075-37-7
Formula : C6H10N2O
M.W : 126.16
SMILES Code : N#CN1CCC(O)CC1
MDL No. :MFCD13178812

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Application In Synthesis of [ 51075-37-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 51075-37-7 ]

[ 51075-37-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 506-68-3 ]
  • [ 5382-17-2 ]
  • [ 51075-37-7 ]
YieldReaction ConditionsOperation in experiment
With sodium carbonate; In dichloromethane; water; at 0℃; for 1.08333h; Preparation 11: 4-Hydroxypiperidine-l-carbonitrileA stirred slurry OfNa2CO3 (9.8 g, 117 mmol) in water (15 mL) was cooled on ice-water and 4-hydroxypiperidine.HCl (4.0 g, 29.2 mmol) was added. A solution of cyanogen bromide(3.7 g, 35 mmol) in CH2Cl2 (90 mL) was added portionwise over 5 min and the stirring continued for 1 h. The reaction was diluted with CH2Cl2 ( 100 mL), the organic phase separated and dried (MgSO-O and the solvent evaporated to afford the title cyanamide: SH (CDCl3) 1.65 (ddt, 2H), 1.91 (ddt, 2H), 2.17 (br s, IH), 3.08 (ddd, 2H), 3.45 (ddd, 2H), 3.86 (sept, IH).
 

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