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[ CAS No. 5250-72-6 ] {[proInfo.proName]}

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Chemical Structure| 5250-72-6
Chemical Structure| 5250-72-6
Structure of 5250-72-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 5250-72-6 ]

CAS No. :5250-72-6 MDL No. :MFCD00111296
Formula : C6H7Cl2N3O4S2 Boiling Point : -
Linear Structure Formula :- InChI Key :DNBXGTICJYDFDT-UHFFFAOYSA-N
M.W : 320.17 Pubchem ID :2781602
Synonyms :

Safety of [ 5250-72-6 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 5250-72-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5250-72-6 ]

[ 5250-72-6 ] Synthesis Path-Downstream   1~51

  • 1
  • [ 5250-72-6 ]
  • [ 50-00-0 ]
  • [ 5233-42-1 ]
YieldReaction ConditionsOperation in experiment
In acetone
With hydrogenchloride In ethanol
In methanol; water for 4h; Heating;
  • 2
  • [ 5250-72-6 ]
  • [ 90150-77-9 ]
YieldReaction ConditionsOperation in experiment
With ammonia In ethanol at 170 - 180℃;
  • 3
  • [ 5250-72-6 ]
  • [ 499-83-2 ]
  • 6-(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-pyridine-2-carboxylic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine at 4℃; for 16h;
  • 4
  • [ 5250-72-6 ]
  • [ 4530-20-5 ]
  • [(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-carbamic acid <i>tert</i>-butyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃;
  • 5
  • [ 5250-72-6 ]
  • [ 13734-36-6 ]
  • [(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-methyl-carbamic acid <i>tert</i>-butyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃;
  • 6
  • [ 5250-72-6 ]
  • [ 31972-52-8 ]
  • ([(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamic acid <i>tert</i>-butyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃;
  • 7
  • [ 5250-72-6 ]
  • C23H23N3O2S [ No CAS ]
  • C29H28Cl2N6O5S3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃;
  • 8
  • [ 5250-72-6 ]
  • [ 18704-37-5 ]
  • 4,5-dichloro-6-(quinoline-8-sulfonylamino)-benzene-1,3-disulfonic acid diamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
90% With triethylamine In acetonitrile at 4℃;
  • 9
  • [ 5250-72-6 ]
  • [ 3303-84-2 ]
  • [2-(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-ethyl]-carbamic acid <i>tert</i>-butyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃;
  • 10
  • [ 5250-72-6 ]
  • [ 873-58-5 ]
  • [ 729-46-4 ]
  • C11H14Cl2N4O5S4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; sodium hypochlorite at 25 - 30℃;
  • 11
  • [ 5250-72-6 ]
  • [ 57294-38-9 ]
  • [3-(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-propyl]-carbamic acid <i>tert</i>-butyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃;
  • 12
  • [ 5250-72-6 ]
  • 1-carboxymethyl-2,4,6-trimethyl-pyridinium; perchlorate [ No CAS ]
  • 1-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-2,4,6-trimethyl-pyridinium; perchlorate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃; for 10h;
  • 13
  • [ 5250-72-6 ]
  • 1-carboxymethyl-2,6-dimethyl-4-phenyl-pyridinium; perchlorate [ No CAS ]
  • 1-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-2,6-dimethyl-4-phenyl-pyridinium; perchlorate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃; for 10h;
  • 14
  • [ 5250-72-6 ]
  • 1-carboxymethyl-2,6-diethyl-4-phenyl-pyridinium; perchlorate [ No CAS ]
  • 1-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-2,6-diethyl-4-phenyl-pyridinium; perchlorate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃; for 10h;
  • 15
  • [ 5250-72-6 ]
  • 1-carboxymethyl-2,6-diisopropyl-4-phenyl-pyridinium; perchlorate [ No CAS ]
  • 1-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-2,6-diisopropyl-4-phenyl-pyridinium; perchlorate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃; for 10h;
  • 16
  • [ 5250-72-6 ]
  • [ 423-60-9 ]
  • 4,5-dichloro-6-(heptadecafluorooctane-1-sulfonylamino)-benzene-1,3-disulfonic acid diamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With pyridine at 20℃;
  • 17
  • [ 5250-72-6 ]
  • [ 421-83-0 ]
  • 4,5-dichloro-6-trifluoromethanesulfonylamino-benzene-1,3-disulfonic acid diamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With pyridine at 20℃;
  • 18
  • [ 5250-72-6 ]
  • [ 2251-50-5 ]
  • <i>N</i>-(2,3-dichloro-4,6-disulfamoyl-phenyl)-2,3,4,5,6-pentafluoro-benzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With pyridine at 20℃;
  • 19
  • [ 5250-72-6 ]
  • [ 832-53-1 ]
  • 4,5-dichloro-6-pentafluorobenzenesulfonylamino-benzene-1,3-disulfonic acid diamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With pyridine at 20℃;
  • 20
  • [ 5250-72-6 ]
  • [ 2991-84-6 ]
  • 4,5-dichloro-6-(nonafluorobutane-1-sulfonylamino)-benzene-1,3-disulfonic acid diamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With pyridine at 20℃;
  • 21
  • [ 5250-72-6 ]
  • [ 52447-23-1 ]
  • 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-nonanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With pyridine at 20℃;
  • 22
  • [ 5250-72-6 ]
  • [ 23911-26-4 ]
  • {{2-[carboxymethyl-(2-{carboxymethyl-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-ethyl)-amino]-ethyl}-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
In N,N-dimethyl-formamide at 20℃; for 4h;
With N,N-dimethyl-formamide at 20℃; for 4h;
  • 23
  • [ 5250-72-6 ]
  • [ 67-43-6 ]
  • [(2-[2-(bis-carboxymethyl-amino)-ethyl]-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-ethyl)-carboxymethyl-amino]-acetic acid [ No CAS ]
  • {(2-[2-(bis-carboxymethyl-amino)-ethyl]-carboxymethyl-amino}-ethyl)-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
1: 80 % Turnov. 2: 20 % Turnov. With diisopropyl-carbodiimide In acetone at 20℃; Title compound not separated from byproducts;
  • 24
  • [ 5250-72-6 ]
  • [ 2936-08-5 ]
  • 2-propyl-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine In acetonitrile at 20℃;
  • 25
  • [ 5250-72-6 ]
  • [ 99-66-1 ]
  • 2-propyl-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 4℃;
  • 26
  • [ 5250-72-6 ]
  • [ 23911-25-3 ]
  • {(2-{carboxymethyl-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-ethyl)-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
  • 27
  • [ 5250-72-6 ]
  • [ 139-13-9 ]
  • {carboxymethyl-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: 4-amino-5,6-dichloro-benzene-1,3-disulfonic acid diamide; nitrilotriacetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetone at 20℃; for 0.25h; Stage #2: With triethylamine In acetone at 4℃; Further stages.;
  • 28
  • [ 5250-72-6 ]
  • [ 60-00-4 ]
  • [2-(bis-carboxymethyl-amino)-ethyl]-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: 4-amino-5,6-dichloro-benzene-1,3-disulfonic acid diamide; ethylenediaminetetraacetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetone at 20℃; for 0.25h; Stage #2: With triethylamine In acetone at 4℃; Further stages.;
  • 29
  • [ 5250-72-6 ]
  • [ 67-42-5 ]
  • {(2-{2-[2-(bis-carboxymethyl-amino)-ethoxy]-ethoxy}-ethyl)-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
  • 30
  • [ 5250-72-6 ]
  • [ 67-43-6 ]
  • {(2-[2-(bis-carboxymethyl-amino)-ethyl]-carboxymethyl-amino}-ethyl)-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: 4-amino-5,6-dichloro-benzene-1,3-disulfonic acid diamide; diethylenetriaminopentaacetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetone at 20℃; for 0.25h; Stage #2: With triethylamine In acetone at 4℃; Further stages.;
  • 31
  • [ 5250-72-6 ]
  • [ 81-23-2 ]
  • (R)-4-((5S,8R,9S,10S,13R,14S,17R)-10,13-Dimethyl-3,7,12-trioxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
  • 32
  • [ 5250-72-6 ]
  • [ 56074-20-5 ]
  • {<i>tert</i>-butoxycarbonyl-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: 4-amino-5,6-dichloro-benzene-1,3-disulfonic acid diamide; N-((tert-butyloxy)carbonyl)iminodiacetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetone at 20℃; for 0.25h; Stage #2: With triethylamine In acetone at 4℃; Further stages.;
  • 33
  • [ 5250-72-6 ]
  • [ 91509-47-6 ]
  • (R)-4-[(3R,5R,8R,9S,10S,13R,14S,17R)-3-(tert-Butyl-dimethyl-silanyloxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃;
  • 34
  • [ 5250-72-6 ]
  • [ 23910-62-5 ]
  • {{2-[2-(2-{carboxymethyl-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-ethoxy)-ethoxy]-ethyl}-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
With N,N-dimethyl-formamide at 20℃; for 4h;
  • 35
  • [ 5250-72-6 ]
  • [ 53049-03-9 ]
  • [<i>tert</i>-butoxycarbonyl-(2-{<i>tert</i>-butoxycarbonyl-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-ethyl)-amino]-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: 4-amino-5,6-dichloro-benzene-1,3-disulfonic acid diamide; N,N'-bis(tert-butoxycarbonyl)ethylenediamine-N'N'-diacetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetone at 20℃; for 0.25h; Stage #2: With triethylamine In acetone at 4℃; Further stages.;
  • 36
  • [ 5250-72-6 ]
  • ((2-<i>tert</i>-butoxycarbonyloxy-phenyl)-{2-[(2-<i>tert</i>-butoxycarbonyloxy-phenyl)-carboxymethyl-amino]-ethyl}-amino)-acetic acid [ No CAS ]
  • [(2-<i>tert</i>-butoxycarbonyloxy-phenyl)-(2-{(2-<i>tert</i>-butoxycarbonyloxy-phenyl)-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-ethyl)-amino]-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: 4-amino-5,6-dichloro-benzene-1,3-disulfonic acid diamide; ((2-<i>tert</i>-butoxycarbonyloxy-phenyl)-{2-[(2-<i>tert</i>-butoxycarbonyloxy-phenyl)-carboxymethyl-amino]-ethyl}-amino)-acetic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetone at 20℃; for 0.25h; Stage #2: With triethylamine In acetone at 4℃; Further stages.;
  • 37
  • [ 5250-72-6 ]
  • [ 250224-37-4 ]
  • (R)-4-[(3R,5S,7R,8R,9S,10S,13R,14S,17R)-3,7-Bis-(tert-butyl-dimethyl-silanyloxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃;
  • 38
  • [ 5250-72-6 ]
  • [ 234447-34-8 ]
  • (R)-4-[(3R,5S,7S,8R,9S,10S,13R,14S,17R)-3,7-Bis-(tert-butyl-dimethyl-silanyloxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃;
  • 39
  • [ 5250-72-6 ]
  • [ 250224-38-5 ]
  • (R)-4-[(3R,5R,8R,9S,10S,12S,13R,14S,17R)-3,12-Bis-(tert-butyl-dimethyl-silanyloxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃;
  • 40
  • [ 5250-72-6 ]
  • [ 164022-54-2 ]
  • (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-3,7,12-Tris-(tert-butyl-dimethyl-silanyloxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentanoic acid (2,3-dichloro-4,6-disulfamoyl-phenyl)-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃;
  • 41
  • [ 5250-72-6 ]
  • [(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: EDCI*HCl / acetone / 0.25 h / 20 °C 1.2: triethylamine / acetone / 4 °C 2.1: trifluoroacetic acid / CH2Cl2 / 0.17 h / 0 °C
  • 42
  • [ 5250-72-6 ]
  • (2-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-amino}-ethylamino)-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: EDCI*HCl / acetone / 0.25 h / 20 °C 1.2: triethylamine / acetone / 4 °C 2.1: trifluoroacetic acid / CH2Cl2 / 0.17 h / 0 °C
  • 43
  • [ 5250-72-6 ]
  • [{2-[[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-(2-hydroxy-phenyl)-amino]-ethyl}-(2-hydroxy-phenyl)-amino]-acetic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: EDCI*HCl / acetone / 0.25 h / 20 °C 1.2: triethylamine / acetone / 4 °C 2.1: trifluoroacetic acid / CH2Cl2 / 0.17 h / 0 °C
  • 44
  • [ 5250-72-6 ]
  • 3-amino-<i>N</i>-(2,3-dichloro-4,6-disulfamoyl-phenyl)-propionamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: EDCI*HCl; Et3N / acetonitrile / 4 °C 2: trifluoroacetic acid / CH2Cl2 / 0.17 h / 0 °C
  • 45
  • [ 5250-72-6 ]
  • 2-amino-<i>N</i>-(2,3-dichloro-4,6-disulfamoyl-phenyl)-acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1-ethyl-3-[3-(dimethylamino)propyl]-carbodiimide*HCl; Et3N / acetonitrile / 4 °C 2: TFA / CH2Cl2 / 0.17 h / 0 °C
  • 46
  • [ 5250-72-6 ]
  • <i>N</i>-(2,3-dichloro-4,6-disulfamoyl-phenyl)-2-methylamino-acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1-ethyl-3-[3-(dimethylamino)propyl]-carbodiimide*HCl; Et3N / acetonitrile / 4 °C 2: TFA / CH2Cl2 / 0.17 h / 0 °C
  • 47
  • [ 5250-72-6 ]
  • 2-amino-<i>N</i>-[(2,3-dichloro-4,6-disulfamoyl-phenylcarbamoyl)-methyl]-acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1-ethyl-3-[3-(dimethylamino)propyl]-carbodiimide*HCl; Et3N / acetonitrile / 4 °C 2: TFA / CH2Cl2 / 0.17 h / 0 °C
  • 48
  • [ 5250-72-6 ]
  • <i>N</i>-(2,3-dichloro-4,6-disulfamoyl-phenyl)-2-(<i>N</i>-methyl-guanidino)-acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1-ethyl-3-[3-(dimethylamino)propyl]-carbodiimide*HCl; Et3N / acetonitrile / 4 °C 2: 4 M HCl / dioxane / 40 °C
  • 49
  • [ 5250-72-6 ]
  • [ 89981-88-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: aq. ethanol / Heating 2: NaBH4 / tetrahydrofuran / Heating
  • 50
  • [ 5250-72-6 ]
  • [ 5625-04-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: NH3 / ethanol / 170 - 180 °C 2: 2-methoxy-ethanol / Heating
  • 51
  • [ 5250-72-6 ]
  • [ 89938-09-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: aq. H2O2, H2SO4 2: methanol / Heating
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