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[ CAS No. 53173-70-9 ]

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Chemical Structure| 53173-70-9
Chemical Structure| 53173-70-9
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Product Details of [ 53173-70-9 ]

CAS No. :53173-70-9 MDL No. :MFCD00720656
Formula : C8H6F2O3 Boiling Point : 276.2±35.0°C at 760 mmHg
Linear Structure Formula :- InChI Key :-
M.W :188.13 g/mol Pubchem ID :21176491
Synonyms :

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Signal Word:Warning Class:N/A
Precautionary Statements:P273-P305+P351+P338 UN#:N/A
Hazard Statements:H319-H412 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 53173-70-9 ]

  • Downstream synthetic route of [ 53173-70-9 ]

[ 53173-70-9 ] Synthesis Path-Downstream   1~2

YieldReaction ConditionsOperation in experiment
PREPARATION 20 3-(Difluoromethoxy)-4-hydroxybenzaldehyde The title compound is prepared according to the reaction procedure of Preparation 19. The title product was isolated from the reaction mixture by column chromatography. M.P.: 64-66 C. NMR (300 MHz, CDCl3): delta6.61 (1H, t), delta9.83 (1H, s).
  • 2
  • [ 53173-70-9 ]
  • [ 139756-02-8 ]
  • [ 1393119-47-5 ]
YieldReaction ConditionsOperation in experiment
88% With indium(III) chloride; In acetonitrile; at 20.0℃; for 1.25h; General procedure: To a solution of aromatic aldehydes 8 (1.0 mmol) in acetonitrile, 4-amino-1-methyl-3-propyl-1H-pyrazole-5-carboxamide 10 (1.0 mmol) and InCl3 (10 mol%) were added at room temparature and the reaction mixture was stirred till the completion of the starting materials (indicated by TLC). The solvent was evoparated and the crude product was triturated with 10% diethyl ether in hexane to obtain the pure product. The product was identified by 1H NMR, 13 C NMR and Mass.
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