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[ CAS No. 546-44-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 546-44-1
Chemical Structure| 546-44-1
Structure of 546-44-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 546-44-1 ]

CAS No. :546-44-1 MDL No. :MFCD01074477
Formula : C13H26O2Si3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 298.60 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 546-44-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 546-44-1 ]

[ 546-44-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 402-43-7 ]
  • [ 546-44-1 ]
  • [ 398-36-7 ]
YieldReaction ConditionsOperation in experiment
96% With tetrabutyl ammonium fluoride In tetrahydrofuran; water at 100℃; for 16h;
With tetrabutyl ammonium fluoride In tetrahydrofuran; water at 100℃; for 16h;
  • 2
  • [ 13688-55-6 ]
  • [ 18052-93-2 ]
  • [ 999-55-3 ]
  • [ 546-44-1 ]
YieldReaction ConditionsOperation in experiment
89.2% With ammonium trifluoromethanesulfonate; 4-methoxy-phenol In hexane at 60℃; for 8h; 3.2 Synthesis of allyl acrylate To a 1L with a constant pressure funnel, a magnetic stir bar, a thermometer and a distillation unitThree bottles were added with 289 g (2.0 mole)Acryloyloxytrimethylsilane, 246 g (1.05 mole)Methylphenyl diallyloxysilane,5.9 g MEHQ,0.55 g of ammonium trifluoromethanesulfonate was added and stirred at 60 ° C for 8 hours, then concentrated under reduced pressure at a low temperature of -20 ° C,A fraction of 201 g was obtained at a yield of 46 to 47 ° C in a yield of 89.2%. The reaction was as shown in formula (12)
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