There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
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CAS No. : | 54704-34-6 | MDL No. : | MFCD08452589 |
Formula : | C9H19N | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 141.25 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Danger | Class: | 3,8 |
Precautionary Statements: | P210-P233-P240-P241-P242-P243-P260-P264-P270-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P370+P378-P403+P235-P405-P501 | UN#: | 2733 |
Hazard Statements: | H226-H302-H314 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Stage #1: L-1-methyl-2-cyclohexylethylamine; 2-(2-formyl-phenoxy)-N-methyl-acetamide In methanol at 100℃; for 2h; Stage #2: With methanol; sodium tetrahydroborate at 60℃; for 6h; | 7.B Step B Aldehyde 3 (0.55 mmol), amine 4 (0.5 mmol) were dissolved in 0.6 ml MeOH, heated at 100° C for 2 hours, then mixture was cooled, NaBH4 (0.5 mmol) was added and stirred for 4 hours. The mixture was heated for 2 hours at 60° C, 3 ml of methanol and 0.2 g of C-18 chromatographic phase were added, stirred for 2 hours, filtered, evaporated and optionally dissolved in 0.5 mL of DMSO. The residue was purified using HPLC. Yield: 24- 47%. (0743) [00304] 8.56 (s, 1H), (0744) 7.19 (t, J = 8.0 Hz, 2H), 6.93 - 6.84 (m, 2H), 4.51 (s, 2H), 3.78 (d, J = 12.0 Hz, 1H), 3.65 (d, J = 12.1 Hz, 1H), 2.71 (d, J = 5.8 Hz, 2H), 2.66 (d, J = 4.6 Hz, 3H), 2.54 (s, 1H), 1.67 (d, J = 15.3 Hz, 5H), 1.35 (s, 1H), 1.20 (dd, J = 22.0, 9.6 Hz, 2H), 1.05 (d, J = 6.2 Hz, 3H), 0.86 (d, J = 12.3 Hz, 2H). |
A583689[ 5471-54-5 ]
1-Cyclohexylpropan-2-amine hydrochloride
Reason: Free-salt