Home Cart 0 Sign in  

[ CAS No. 5577-13-9 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 5577-13-9
Chemical Structure| 5577-13-9
Structure of 5577-13-9 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 5577-13-9 ]

Related Doc. of [ 5577-13-9 ]

Alternatived Products of [ 5577-13-9 ]

Product Details of [ 5577-13-9 ]

CAS No. :5577-13-9 MDL No. :MFCD00797861
Formula : C10H13NO4S Boiling Point : -
Linear Structure Formula :- InChI Key :DFWQXANLGSXMKF-UHFFFAOYSA-N
M.W : 243.28 Pubchem ID :79683
Synonyms :
Chemical Name :Ethyl N-(4-methylbenzenesulfonyl)carbamate

Safety of [ 5577-13-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H332-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 5577-13-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 5577-13-9 ]
  • Downstream synthetic route of [ 5577-13-9 ]

[ 5577-13-9 ] Synthesis Path-Upstream   1~11

  • 1
  • [ 541-41-3 ]
  • [ 70-55-3 ]
  • [ 5577-13-9 ]
Reference: [1] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2008, vol. 71, # 2, p. 523 - 528
[2] Chemical and Pharmaceutical Bulletin, 2008, vol. 56, # 4, p. 541 - 546
[3] Patent: DE1011414, 1955, ,
[4] Journal of Organic Chemistry, 1971, vol. 36, p. 4102 - 4105
[5] Patent: DE1011414, 1953, ,
[6] Patent: DE965400, 1955, ,
  • 2
  • [ 64-17-5 ]
  • [ 31224-37-0 ]
  • [ 5577-13-9 ]
YieldReaction ConditionsOperation in experiment
84% at 120℃; for 0.333333 h; Sealed tube; Microwave irradiation General procedure: The 4-substituted methyl (phenylsulfonyl)carbamate was dissolved in the chosen alcohol (2 mL) in a microwave vial, which was closed using an aluminum open-top seal with PTFE-faced septum. The reaction mixture was heated under microwave irradiation at 100-120 oC for 20-60 min. The crude reaction mixture was concentrated under reduced pressure and the residue was purified using silica gel column chromatography to yield the desired (aryl)carbamate.
Reference: [1] Tetrahedron Letters, 2016, vol. 57, # 13, p. 1476 - 1478
  • 3
  • [ 941-55-9 ]
  • [ 64-17-5 ]
  • [ 201230-82-2 ]
  • [ 5577-13-9 ]
Reference: [1] Angewandte Chemie - International Edition, 2016, vol. 55, # 18, p. 5545 - 5549[2] Angew. Chem., 2016, vol. 128, # 18, p. 5635 - 5639,5
  • 4
  • [ 4083-64-1 ]
  • [ 5577-13-9 ]
Reference: [1] Patent: US5326796, 1994, A,
[2] Patent: US5326796, 1994, A,
[3] Patent: US5326796, 1994, A,
[4] Patent: US5326796, 1994, A,
[5] Patent: US5326796, 1994, A,
[6] Patent: US5326796, 1994, A,
[7] Patent: US5326796, 1994, A,
[8] Patent: US5326796, 1994, A,
[9] Patent: US5326796, 1994, A,
[10] Patent: US5326796, 1994, A,
  • 5
  • [ 5219-81-8 ]
  • [ 105-58-8 ]
  • [ 5577-13-9 ]
Reference: [1] Synthetic Communications, 2011, vol. 41, # 8, p. 1102 - 1111
  • 6
  • [ 70-55-3 ]
  • [ 1608-26-0 ]
  • [ 5577-13-9 ]
Reference: [1] Journal of Organic Chemistry, 1985, vol. 50, # 10, p. 1712 - 1718
  • 7
  • [ 70-55-3 ]
  • [ 5577-13-9 ]
Reference: [1] Tetrahedron Letters, 2016, vol. 57, # 13, p. 1476 - 1478
[2] Tetrahedron Letters, 2016, vol. 57, # 13, p. 1476 - 1478
  • 8
  • [ 10439-23-3 ]
  • [ 5577-13-9 ]
Reference: [1] J. Gen. Chem. USSR (Engl. Transl.), 1961, vol. 31, p. 2218 - 2222[2] Zhurnal Obshchei Khimii, 1961, vol. 31, p. 2381 - 2385
  • 9
  • [ 98-59-9 ]
  • [ 5577-13-9 ]
Reference: [1] Angewandte Chemie - International Edition, 2016, vol. 55, # 18, p. 5545 - 5549[2] Angew. Chem., 2016, vol. 128, # 18, p. 5635 - 5639,5
  • 10
  • [ 93506-31-1 ]
  • [ 5577-13-9 ]
Reference: [1] J. Gen. Chem. USSR (Engl. Transl.), 1961, vol. 31, p. 2218 - 2222[2] Zhurnal Obshchei Khimii, 1961, vol. 31, p. 2381 - 2385
  • 11
  • [ 14437-03-7 ]
  • [ 5577-13-9 ]
Reference: [1] Tetrahedron Letters, 2016, vol. 57, # 13, p. 1476 - 1478
Recommend Products
Same Skeleton Products
Historical Records

Related Functional Groups of
[ 5577-13-9 ]

Aryls

Chemical Structure| 14437-03-7

[ 14437-03-7 ]

Methyl tosylcarbamate

Similarity: 0.96

Chemical Structure| 1694-06-0

[ 1694-06-0 ]

N-Carbamoyl-4-methylbenzenesulfonamide

Similarity: 0.74

Chemical Structure| 640-61-9

[ 640-61-9 ]

N,4-Dimethylbenzenesulfonamide

Similarity: 0.73

Chemical Structure| 318515-70-7

[ 318515-70-7 ]

Ethyl (4-(2-(3-ethyl-4-methyl-2-oxo-2,5-dihydro-1H-pyrrole-1-carboxamido)ethyl)phenyl)sulfonylcarbamate

Similarity: 0.69

Chemical Structure| 7326-73-0

[ 7326-73-0 ]

3-(N,N-Dimethylsulfamoyl)benzoic acid

Similarity: 0.68

Amides

Chemical Structure| 14437-03-7

[ 14437-03-7 ]

Methyl tosylcarbamate

Similarity: 0.96

Chemical Structure| 1694-06-0

[ 1694-06-0 ]

N-Carbamoyl-4-methylbenzenesulfonamide

Similarity: 0.74

Chemical Structure| 318515-70-7

[ 318515-70-7 ]

Ethyl (4-(2-(3-ethyl-4-methyl-2-oxo-2,5-dihydro-1H-pyrrole-1-carboxamido)ethyl)phenyl)sulfonylcarbamate

Similarity: 0.69

Chemical Structure| 6971-74-0

[ 6971-74-0 ]

N-Tosylbenzamide

Similarity: 0.65

Chemical Structure| 144-80-9

[ 144-80-9 ]

N-((4-Aminophenyl)sulfonyl)acetamide

Similarity: 0.63

Amines

Chemical Structure| 14437-03-7

[ 14437-03-7 ]

Methyl tosylcarbamate

Similarity: 0.96

Chemical Structure| 1694-06-0

[ 1694-06-0 ]

N-Carbamoyl-4-methylbenzenesulfonamide

Similarity: 0.74

Chemical Structure| 640-61-9

[ 640-61-9 ]

N,4-Dimethylbenzenesulfonamide

Similarity: 0.73

Chemical Structure| 318515-70-7

[ 318515-70-7 ]

Ethyl (4-(2-(3-ethyl-4-methyl-2-oxo-2,5-dihydro-1H-pyrrole-1-carboxamido)ethyl)phenyl)sulfonylcarbamate

Similarity: 0.69

Chemical Structure| 7326-73-0

[ 7326-73-0 ]

3-(N,N-Dimethylsulfamoyl)benzoic acid

Similarity: 0.68

Sulfamides

Chemical Structure| 14437-03-7

[ 14437-03-7 ]

Methyl tosylcarbamate

Similarity: 0.96

Chemical Structure| 1694-06-0

[ 1694-06-0 ]

N-Carbamoyl-4-methylbenzenesulfonamide

Similarity: 0.74

Chemical Structure| 640-61-9

[ 640-61-9 ]

N,4-Dimethylbenzenesulfonamide

Similarity: 0.73

Chemical Structure| 318515-70-7

[ 318515-70-7 ]

Ethyl (4-(2-(3-ethyl-4-methyl-2-oxo-2,5-dihydro-1H-pyrrole-1-carboxamido)ethyl)phenyl)sulfonylcarbamate

Similarity: 0.69

Chemical Structure| 7326-73-0

[ 7326-73-0 ]

3-(N,N-Dimethylsulfamoyl)benzoic acid

Similarity: 0.68