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[ CAS No. 59-63-2 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 59-63-2
Chemical Structure| 59-63-2
Structure of 59-63-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 59-63-2 ]

CAS No. :59-63-2 MDL No. :MFCD00865409
Formula : C12H13N3O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 231.25 Pubchem ID :-
Synonyms :
NSC 169893;Ro 5-0831

Safety of [ 59-63-2 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P301+P310 UN#:2811
Hazard Statements:H301 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 59-63-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 59-63-2 ]

[ 59-63-2 ] Synthesis Path-Downstream   1~9

  • 2
  • [ 39499-34-8 ]
  • [ 59-63-2 ]
  • [ 101670-68-2 ]
YieldReaction ConditionsOperation in experiment
In diethyl ether
  • 3
  • [ 91397-11-4 ]
  • [ 59-63-2 ]
YieldReaction ConditionsOperation in experiment
With potassium borohydride In methanol; water
339 mg Stage #1: 5-methyl-isoxazole-3-carboxylic acid benzylidenehydrazide With borane pyridine; acetic acid at 0℃; for 0.0833333h; Stage #2: With hydrogenchloride In water at 0 - 20℃; for 0.5h; N′-Benzyl-5-methylisoxazole-3-carbohydrazide (3, Isocarboxazid) To a stirred solution of 5-methylisoxazole-3-carbohydrazide (15;265 mg, 1.88 mmol) in MeOH (3 mL) was added a solution of benzaldehyde(200 mg, 1.88 mmol) in MeOH (2 mL) under an atmosphere of N2 and the mixture was stirred for 10 min at r.t. After cooling to 0 °C, AcOH (0.5 mL) and α-PicBH3 (201 mg, 1.88mmol) were added and the mixture was stirred for 5 min at the same temperature. To the mixture was added 3 M aq HCl (2.51 mL, 7.52mmol) at 0 °C, and was allowed to warm to r.t. After stirring for 30 min, the mixture was poured into 25% aq Na2CO3 (10 mL) and extracted with EtOAc (3 × 20 mL). The combined organic layers were washed with brine, dried (MgSO4), filtered, and the filtrate was concentrated in vacuo. The residue was purified by silica gel column chromatography (n-hexane-EtOAc, 9:1) to give 3; yield: 339 mg(83%); colorless crystals: mp 105-106 °C.
YieldReaction ConditionsOperation in experiment
Cer(IV)-sulfat/aq.H2SO4 (Raumtemp.) -> 5-Methylisoxazol-3-carbonsaeure, Benzylal-kohol, Benzaldehyd;
Farbreaktion m. Nitroprussid-Na;
Rk. mit Hydrazin -> 5-(2-Phenyl-hydrazino-carbonyl)-imidazol-4-carbonsaeure-hydrazid, analoge Rk. mit Hydrazinderiv.;
  • 5
  • [ 62438-03-3 ]
  • [ 59-63-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: ethanol 2: KBH4 / methanol; H2O
  • 6
  • [ 100-52-7 ]
  • [ 59-63-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: ethanol 2: KBH4 / methanol; H2O
  • 7
  • [ 19788-35-3 ]
  • [ 20570-96-1 ]
  • [ 59-63-2 ]
YieldReaction ConditionsOperation in experiment
93% With triethylamine; In n-heptane; at 35℃; A reactor was charged at room temperature with methyl 5-methylisoxazole-3-carboxylate (30g), <strong>[20570-96-1]benzylhydrazine dihydrochloride</strong> (62.8 g, potentiometric assay of 99%) and n-heptane(450 ml). To the suspension was added slowly with a dropping funnel triethylamine (65.6 g).At the end of the addition the temperature was adjusted to about 35C and maintained at thattemperature overnight. An in-process control sample taken after about 16 hours showed only 0.2% of methyl 5-methylisoxazole-3-carboxylate. The suspension was cooled to 20C and water (120 ml) was added slowly with a dropping funnel. The suspension was filtered and washed with water (2 x 60 ml) and n-heptane (2 x 60 ml). The product was dried undervacuum at 50C and Isocarboxazid (45.5 g, molar yield of 93%, purity by HPLC 99.1%) was obtained as white solid.
  • 8
  • [ 59-63-2 ]
  • [ 2469-99-0 ]
  • N-(benzylamino)isocyanate [ No CAS ]
  • 9
  • [ 59-63-2 ]
  • [ 491594-42-4 ]
YieldReaction ConditionsOperation in experiment
In N,N-dimethyl-formamide at 150℃; Inert atmosphere;
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