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Chemistry
Organic Building Blocks
Aryls
2-(3,4-Dimethoxyphenyl)acetohydrazide
Chemistry
Organic Building Blocks
Aryls
Amines Amides Ethers Hydrazines Hydrazides Benzene Compounds

[ CAS No. 60075-23-2 ]

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Cat. No.: {[proInfo.prAm]}
3d Animation Molecule Structure of 60075-23-2
Chemical Structure| 60075-23-2
Chemical Structure| 60075-23-2
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Quality Control of [ 60075-23-2 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 60075-23-2 ]

SDS Specification
Alternatived Products of [ 60075-23-2 ]

Product Details of [ 60075-23-2 ]

CAS No. :60075-23-2 MDL No. :MFCD00051701
Formula : C10H14N2O3 Boiling Point : -
Linear Structure Formula :- InChI Key :HRMXYTRKEOUMNG-UHFFFAOYSA-N
M.W :210.23 Pubchem ID :282482
Synonyms :

Safety of [ 60075-23-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280 UN#:N/A
Hazard Statements:H302-H312-H332 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 60075-23-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60075-23-2 ]

[ 60075-23-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 18066-68-7 ]
  • [ 60075-23-2 ]
Reference： [1]Journal of the Chemical Society,1930,p. 2354,2356
[2]Acta poloniae pharmaceutica,2009,vol. 66,p. 73 - 82
  • 2
  • [ 15964-79-1 ]
  • [ 60075-23-2 ]
YieldReaction ConditionsOperation in experiment
With pyridine; hydrazine hydrate; In ethanol; for 10h;Reflux; General procedure: To a mixture corresponding ester (9a-n, 5.0 mmol) and hydrazine monohydrate (15.0 mmol) in ethanol, catalytic amount of pyridine (0.5 mL) was added and refluxed for 10 h. The reaction was monitored by TLC. After the completion of the reaction, ethanol was evaporated from the mixture, water was added and extracted using ethyl acetate. The organic layer was dried over anhydrous sodium sulfate and evaporated under vacuum to get the crude mass. Finally, the products 10a-n were purified using column chromatography. (Yield 80-85%).
Reference： [1]Journal of the Chemical Society. Perkin Transactions 1 (2001),2002,p. 513 - 528
[2]Bioorganic and Medicinal Chemistry Letters,2018,vol. 28,p. 2369 - 2374
  • 3
  • [ 60075-23-2 ]
  • [ 18496-54-3 ]
  • N'-(2-(3,4-dimethoxyphenyl)acetyl)-4-phenylbutanehydrazide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; at 0℃; for 2h; General procedure: To a cooled solution of the 10a-n (3.0 mmol) in dichloromethane, triethylamine (3.0 mmol) was added at 0 C followed by the addition of the corresponding 12a-c (3.0 mmol). The reaction mixture was stirred at 0 C for 2 h. After the completion of the reaction, water was added and the reaction mixture was extracted using ethyl acetate. The organic layer was washed with 10% sodium bicarbonate solution and finally with brine solution. It was dried over anhydrous sodium sulfate and evaporated under vacuum. The products 13a-q was purified by column chromatography.
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2018,vol. 28,p. 2369 - 2374

Tags: 60075-23-2 synthesis path| 60075-23-2 SDS| 60075-23-2 COA| 60075-23-2 purity| 60075-23-2 application| 60075-23-2 NMR| 60075-23-2 COA| 60075-23-2 structure

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