[ CAS No. 619-26-1 ]

Name: 619-26-1|N-Methyl-3-nitroaniline|98%
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COA NMR CNMR HPLC LC-MS

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SDS Specification

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CAS No. :	619-26-1	MDL No. :	MFCD00963641
Formula :	C₇H₈N₂O₂	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	IKSRCCUOUJJGAU-UHFFFAOYSA-N
M.W :	152.15	Pubchem ID :	219622
Synonyms :

Safety of [ 619-26-1 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P280	UN#:	N/A
Hazard Statements:	H302-H317	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 619-26-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Upstream synthesis route of [ 619-26-1 ]
Downstream synthetic route of [ 619-26-1 ]

[ 619-26-1 ] Synthesis Path-Upstream 1~2

1
[ 201230-82-2 ]
[ 619-26-1 ]
[ 73043-80-8 ]

Reference： [1] Journal of the American Chemical Society, 2012, vol. 134, # 42, p. 17490 - 17493,4

2
[ 619-26-1 ]
[ 50617-73-7 ]

Reference： [1] Chemische Berichte, 1886, vol. 19, p. 550
[2] Rep.sci.Res.Inst.Tokyo, 1949, vol. 25, p. 316,319[3] Chem.Abstr., 1951, p. 7127
[4] Journal of the Chemical Society, 1948, p. 1926,1930
[5] Chemische Berichte, 1886, vol. 19, p. 550

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Yield	Reaction Conditions	Operation in experiment
96%	Stage #1: 3-nitro-aniline With trifluoroacetic anhydride In 1,2-dichloro-ethane at 0℃; for 1h; Stage #2: methyl iodide With potassium carbonate In butanone at 60℃; for 2h; Stage #3: With methanol; potassium carbonate at 20℃; for 1h;
29%	With potassium carbonate In acetone at 50℃;	14.1 Step 1: N-methyl-3-nitroaniline Step 1: N-methyl-3-nitroaniline To a solution of 3-nitrobenzenamine (5 g 36.2 mmol) in acetone (30 mL) were added iodomethane (5.65 g, 39.8 mmol) and potassium carbonate (10 g, 72.4 mmol). The mixture was stirred at 50°C overnight. The mixture was concentrated to dryness under reduced pressure. The residue was purified by column chromatography (petroleum ether:ethylacetate, 10:1) to give N-methyl-3-nitroaniline (1.6 g, 29%) as a red solid. LCMS (Method B): 3.01 mm [MH]= 153.1.
	With sodium hydroxide; ethanol

Yield	Reaction Conditions	Operation in experiment
	at 80℃; for 2h;
	In ethanol at 80℃;

Yield	Reaction Conditions	Operation in experiment
	at 80℃; for 2h;
	In ethanol at 80℃;

Yield	Reaction Conditions	Operation in experiment
	at 80℃; for 2h;
	In ethanol at 80℃;

[ CAS No. 619-26-1 ]

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