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Chemical Structure| 63297-02-9 Chemical Structure| 63297-02-9

Structure of 63297-02-9

Chemical Structure| 63297-02-9

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Product Details of [ 63297-02-9 ]

CAS No. :63297-02-9
Formula : C16H14O4
M.W : 270.28
SMILES Code : O=C(C1=CC=C(C2=CC=C(C(O)=O)C(C)=C2)C=C1C)O
MDL No. :MFCD30542914
InChI Key :KWJNTOJAUQZMJO-UHFFFAOYSA-N
Pubchem ID :11807754

Safety of [ 63297-02-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 63297-02-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 63297-02-9 ]

[ 63297-02-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 84-67-3 ]
  • [ 63297-02-9 ]
  • [ 7583-27-9 ]
YieldReaction ConditionsOperation in experiment
74% e) Synthesis E 3,3'-dimethylbiphenyl-4,4'-dicarboxylic acid The reaction scheme for this synthesis is represented below: The same procedure as that described for synthesis D was used, starting with 12.1 g of dimethylbenzidine. After the first step, 18.4 g of 3,3'-dimethyl-4,4'-diiodobiphenyl are obtained (yield: 74percent). Characterization of the diiodo compound obtained: 1H NMR (300 MHz, CDCl3): delta (ppm): 2.54 (s, 6H), 7.10 (dd, J=2.2 and 8.1 Hz, 2H), 7.46 (d, J=2.2 Hz, 2H), 7.90 (d, J=8.1 Hz, 2H). 13C NMR (75 MHz, CDCl3): delta (ppm): 28.3 (CH3), 100.3 (Cq), 126.0 (CH), 128.3 (CH), 139.4 (CH), 140.4 (Cq), 141.9 (Cq).
 

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