[ CAS No. 6342-17-2 ]

Name: 6342-17-2|1,1'-(Piperazine-1,4-diyl)bis(prop-2-en-1-one)|95%
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SKU: A290897
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Quality Control of [ 6342-17-2 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 6342-17-2 ]

SDS Specification

Alternatived Products of [ 6342-17-2 ]

Product Details of [ 6342-17-2 ]

CAS No. :	6342-17-2	MDL No. :	MFCD00077661
Formula :	C₁₀H₁₄N₂O₂	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	YERHJBPPDGHCRJ-UHFFFAOYSA-N
M.W :	194.23	Pubchem ID :	193422
Synonyms :

Safety of [ 6342-17-2 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 6342-17-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 6342-17-2 ]

[ 6342-17-2 ] Synthesis Path-Downstream 1~15

1
[ 110-85-0 ]
[ 814-68-6 ]
[ 6342-17-2 ]

Yield	Reaction Conditions	Operation in experiment
72%	With triethylamine In dichloromethane Ambient temperature;
70%	In dichloromethane; triethylamine at -5 - 20℃; for 13h;
65%	With triethylamine In dichloromethane 1.) 0 deg C, 739 min; 2.) RT, 1 h;

57%	With triethylamine In dichloromethane at 0 - 20℃; for 1.75h;
55%	With triethylamine

Reference： [1]Taillades, J.; Boussac, P.; Collet, H.; Brugidou, J.; Commeyras, A. [Bulletin de la Societe Chimique de France, 1991, # 3, p. 423 - 429]
[2]Sha, Yaowu; Shen, Liang; Hong, Xiaoyin [Tetrahedron Letters, 2002, vol. 43, # 51, p. 9417 - 9419]
[3]Honnoraty, Anne-Marie; Mion, Louis; Rousset, Alain; Taillades, Jacques; Commeyras, Auguste [Bulletin de la Societe Chimique de France, 1995, vol. 132, # 7, p. 721 - 728]
[4]Mann, Stephane; Carillon, Sophie; Breyne, Olivier; Marquet, Andree [Chemistry - A European Journal, 2002, vol. 8, # 2, p. 439 - 450]
[5]Taillades, Jacques; Garrel, Laurence; Guillen, Franck; Collet, Helene; Commeyras, Auguste [Bulletin de la Societe Chimique de France, 1995, vol. 132, p. 119 - 127]
[6]Sola, R.; Brugidou, J.; Taillades, J.; Commeyras, A.; Previero, A. [Tetrahedron Letters, 1983, vol. 24, # 14, p. 1501 - 1504]

Yield	Reaction Conditions	Operation in experiment
	polymerisiert beim Stehenlassen;
	Polyaddition;
	Rk. mit Propan-2-ol in Ggw. v. KOCH(CH3)2 bei 24grad;

Rk. mit Propan-2-ol (50percent) in N,N-Dimethylformamid in Ggw. v. KOCH(CH3)2 bei 24grad;

Yield	Reaction Conditions	Operation in experiment
	1,4-Bis-(3-chlor-propionyl)-piperazin bei der Chromatographie an Al2O3;
	Acryloylchlorid, Piperazin;
	entspr. Acrylat, 1) Halocarbonat, 2) Piperazin;

The process of claim 1, wherein said polyfunctional compound copolymerizable with acrylamide is selected from the group consisting of ... butylidene bis-acrylamide, benzylidene bis-acrylamide, diacrylamido acetic acid, xylylidene tetra-acrylamide, N,N'-bis-(acrylyl) piperazine and p-benzylidene camphor-N,N'-acrylyl diaminomethane.

4
[ 111-42-2 ]
[ 6342-17-2 ]
[ 497147-13-4 ]

Yield	Reaction Conditions	Operation in experiment
85%	In ethanol at 20℃; for 20h;

Reference： [1]Sha, Yaowu; Shen, Liang; Hong, Xiaoyin [Tetrahedron Letters, 2002, vol. 43, # 51, p. 9417 - 9419]

5
[ 109-07-9 ]
[ 6342-17-2 ]
polymer, M_n 10000 Da, PDI 2.5; monomer(s): 1,4-diacryloylpiperazine; 2-methylpiperazine [ No CAS ]

Reference： [1]Magnetic Resonance in Chemistry,2007,vol. 45,p. 51 - 58

6
[ 109-07-9 ]
[ 107-15-3 ]
[ 6342-17-2 ]
polymer, network, molar feed ratio of diacryloylpiperazine/2-methylpiperazine/ethylenediamine 5.15/4.12/0.515; monomer(s): 1,4-diacryloylpiperazine; 2-methylpiperazine; ethylenediamine [ No CAS ]

Reference： [1]Magnetic Resonance in Chemistry,2007,vol. 45,p. 51 - 58

7
[ 109-07-9 ]
[ 107-15-3 ]
[ 6342-17-2 ]
polymer, network, molar feed ratio of diacryloylpiperazine/2-methylpiperazine/ethylenediamine 5.15/3.10/1.03; monomer(s): 1,4-diacryloylpiperazine; 2-methylpiperazine; ethylenediamine [ No CAS ]

Reference： [1]Magnetic Resonance in Chemistry,2007,vol. 45,p. 51 - 58

8
[ 109-07-9 ]
[ 107-15-3 ]
[ 6342-17-2 ]
polymer, network, molar feed ratio of diacryloylpiperazine/2-methylpiperazine/ethylenediamine 5.15/1.03/2.06; monomer(s): 1,4-diacryloylpiperazine; 2-methylpiperazine; ethylenediamine [ No CAS ]

Reference： [1]Magnetic Resonance in Chemistry,2007,vol. 45,p. 51 - 58

9
[ 6342-17-2 ]
G₁-(acrylate)₄ [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: 85 percent / ethanol / 20 h / 20 °C 2: 79 percent / CH₂Cl₂; triethylamine / 13 h / -5 - 20 °C

Reference： [1]Sha, Yaowu; Shen, Liang; Hong, Xiaoyin [Tetrahedron Letters, 2002, vol. 43, # 51, p. 9417 - 9419]

10
[ 6342-17-2 ]
[ 497147-15-6 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 3 steps 1: 85 percent / ethanol / 20 h / 20 °C 2: 79 percent / CH₂Cl₂; triethylamine / 13 h / -5 - 20 °C 3: 82 percent / ethanol / 20 h / 20 °C

Reference： [1]Sha, Yaowu; Shen, Liang; Hong, Xiaoyin [Tetrahedron Letters, 2002, vol. 43, # 51, p. 9417 - 9419]

11
[ 6342-17-2 ]
[ 178949-82-1 ]
BP-EDDS [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
91.8%	With lithium hydroxide	24 Lithium hydroxide monohydrate (112,64 mg, 2,6576 mmol) was added under stirring to a 37,36% solution (as determined titrimetrically just before use) of EDDS) (2 ml, 2.6576 mmol) contained in a 50 ml 2 necked flask. 1 ,4- bisacryloylpiperazine (BP) (516,19 mg. 2,6576 mmol) was then added. The reaction mixture was then treated and the final product isolated exactly as described in the previous case. Yield 91 ,8 %. M«> = 6500, Mn = 4500.

Reference： [1]Current Patent Assignee: COLOROBBIA HOLDING SPA - WO2008/74804, 2008, A2 Location in patent: Page/Page column 46

12
[ 120737-59-9 ]
[ 6342-17-2 ]
[ 1422359-92-9 ]

Yield	Reaction Conditions	Operation in experiment
75%	In water at 0℃; for 48h;

Reference： [1]Ferruti, Paolo; Mauro, Nicolo; Manfredi, Amedea; Ranucci, Elisabetta [Journal of Polymer Science, Part A: Polymer Chemistry, 2012, vol. 50, # 23, p. 4947 - 4957]

13
[ 6342-17-2 ]
[ 57260-71-6 ]
[ 1422359-91-8 ]

Yield	Reaction Conditions	Operation in experiment
81%	In water at 0℃; for 48h;

Reference： [1]Ferruti, Paolo; Mauro, Nicolo; Manfredi, Amedea; Ranucci, Elisabetta [Journal of Polymer Science, Part A: Polymer Chemistry, 2012, vol. 50, # 23, p. 4947 - 4957]

14
[ 32586-73-5 ]
[ 108-24-7 ]
[ 1696-20-4 ]
[ 6342-17-2 ]

Yield	Reaction Conditions	Operation in experiment
1: 83% 2: 85%	Stage #1: N,N'-bis(morpholinopropionyl)piperazine; acetic anhydride In toluene at 20 - 80℃; for 2h; Inert atmosphere; Stage #2: With 2,6-di-tert-butyl-4-methyl-phenol; triethylamine for 12h; Reflux;	5 Example 5: Under argon atmosphere, 17.8 g of benzyl bromide and 23 g of morpholinopropionyl morpholine were mixed with 250 ml of toluene, and the temperature was gradually increased from room temperature to 60 to 80 degrees Celsius and stirred for 2 hours. After stirring 0.2 grams of inhibitor BHT and 11.1 grams were addedTriethylamine, and gradually warmed to reflux for 12 hours, the reaction system was concentrated under reduced pressure to give the crude product was directly purified by silica gel column chromatographyElution with hexane-ethyl acetate gave 10.8 g of pure (in 77% yield) of acryloylmorpholine and pure N-benzylmorpholine14.9 g (84% yield).

Reference： [1]Current Patent Assignee: SHENZHEN YOUWEI CHEMICAL TECH - CN107417644, 2017, A Location in patent: Paragraph 0017

15
[ 110-85-0 ]
[ 79-10-7 ]
[ 6342-17-2 ]

Yield	Reaction Conditions	Operation in experiment
95%	With (ZrO₂-Fe₃O₄-Nb₂O₅) catalyst In toluene at 60℃; for 6h; Schlenk technique; Inert atmosphere;	4 Example 4 Take a 50mL Schlenk bottle, bake and replace the argon gas, add acrylic acid (1.44g, about 24mmol), piperazine (0.86g, about 10mmol) in 20mL of toluene, and then add the zirconium-based three prepared in Example 1 Metal oxide solid acid (ZrO2-Fe3O4-Nb2O5) (8.6mg), heated to 60°C, stirred for 6h, filtered the catalyst, washed the catalyst with toluene 2 times, and recovered and reused. The filtrate was washed 3 times with a pH 10 NaOH aqueous solution, and after washing with brine to neutrality, the liquid was separated, the organic phase was evaporated to remove the solvent, and dried under vacuum to obtain 1,4-diacryloylpiperazine with a yield of 95%

Reference： [1]Current Patent Assignee: SHANDONG JINZHIRUI NEW MAT DEVELOPMENT - CN113636989, 2021, A Location in patent: Paragraph 0069-0072

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Code	Phrase
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P321
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P342	If experiencing respiratory symptoms:
P350	Gently wash with plenty of soap and water.
P351	Rinse cautiously with water for several minutes.
P352	Wash with plenty of soap and water.
P353	Rinse skin with water/shower.
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P361	Remove/Take off immediately all contaminated clothing.
P362	Take off contaminated clothing and wash before reuse.
P363	Wash contaminated clothing before reuse.
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P372	Explosion risk in case of fire.
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P376	Stop leak if safe to do so. Oxidising gases (section 2.4) 1
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P378
P380	Evacuate area.
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P390	Absorb spillage to prevent material damage.
P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P301 + P312	IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301 + P330 + P331	IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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P410 + P403	Protect from sunlight. Store in a well-ventilated place.
P410 + P412	Protect from sunlight. Do not expose to temperatures exceeding 50 oC/122oF.
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Physical hazards
Code	Phrase
H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
H220	Extremely flammable gas
H221	Flammable gas
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H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
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H290	May be corrosive to metals
Health hazards
Code	Phrase
H300	Fatal if swallowed
H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
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H361d	Suspected of damaging the unborn child
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H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 6342-17-2 ]

Quality Control of [ 6342-17-2 ]

Related Doc. of [ 6342-17-2 ]

Product Details of [ 6342-17-2 ]

Safety of [ 6342-17-2 ]

Application In Synthesis of [ 6342-17-2 ]

[ 6342-17-2 ] Synthesis Path-Downstream 1~15

Related Functional Groups of [ 6342-17-2 ]

Alkenyls

Amides

Related Parent Nucleus of [ 6342-17-2 ]

Piperazines

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

Inquiry

Related Functional Groups of
[ 6342-17-2 ]

Related Parent Nucleus of
[ 6342-17-2 ]