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Chemical Structure| 6342-75-2 Chemical Structure| 6342-75-2

Structure of 6342-75-2

Chemical Structure| 6342-75-2

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Product Details of [ 6342-75-2 ]

CAS No. :6342-75-2
Formula : C10H12O2
M.W : 164.20
SMILES Code : CC(C1=CC=CC(C)=C1OC)=O
English Name :1-(2-Methoxy-3-methylphenyl)ethanone
MDL No. :MFCD11044853

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Application In Synthesis of [ 6342-75-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6342-75-2 ]

[ 6342-75-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 26507-91-5 ]
  • [ 917-54-4 ]
  • [ 6342-75-2 ]
YieldReaction ConditionsOperation in experiment
246.9 mg In diethyl ether at 0 - 20℃; General procedure G (GP G): Ketone formation from carboxylicacid using methyl lithium Adapting the literature-known procedure[53] slightly, a mixture of carboxylic acid and diethyl ether (Et2O, 0.13M) was cooled to 0 C under dry conditions. To this mixture, a solution ofmethyl lithium (MeLi) (1.6 M in Et2O, 4.0 equiv) was added dropwise.The resulting mixture was stirred o/n reaching r. t. and then quenchedwith aqueous, saturated NH4Cl solution. After extraction with DCM, theresulting organic layers were combined, washed with saturated,aqueous NaCl solution and dried over Na2SO4. Lastly, it was filtered anddried in vacuo. The resulting crude was purified by AFC if necessary.
 

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