Alternatived Products of [ 680203-71-8 ]
Product Details of [ 680203-71-8 ]
CAS No. : | 680203-71-8 |
MDL No. : | MFCD09741874 |
Formula : |
C12H18ClNO2
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
243.73
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 680203-71-8 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 680203-71-8 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 680203-71-8 ]
- 1
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[ 1563-38-8 ]
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[ 680203-71-8 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 3 steps
1: K2CO3 / butan-2-one / 22 h / 80 °C
2: 18 g / dimethylformamide / 2 h / Heating
3: ethanolamine / 18 h / 20 °C |
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Multi-step reaction with 2 steps
1.1: potassium carbonate / acetone / 48 h / 50 °C
2.1: potassium phtalimide; 18-crown-6 ether / N,N-dimethyl-formamide / 3 h / 50 °C
2.2: 2 h / 50 °C
2.3: 1 h / 20 °C |
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Multi-step reaction with 3 steps
1.1: potassium carbonate / acetone / 48 h / 50 °C
2.1: 18-crown-6 ether / N,N-dimethyl-formamide / 3 h / 50 °C
3.1: methylamine / water / 2 h / 50 °C
3.2: 1 h / 20 °C |
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Reference:
[1]Cuisiat, Stephane; Bourdiol, Nathalie; Lacharme, Vincent; Newman-Tancredi, Adrian; Colpaert, Francis; Vacher, Bernard
[Journal of Medicinal Chemistry, 2007, vol. 50, # 4, p. 865 - 876]
[2]Sniecikowska, Joanna; Gluch-Lutwin, Monika; Bucki, Adam; Wiȩckowska, Anna; Siwek, Agata; Jastrzebska-Wiesek, Magdalena; Partyka, Anna; Wilczyńska, Daria; Pytka, Karolina; Latacz, Gniewomir; Przejczowska-Pomierny, Katarzyna; Wyska, Elżbieta; Wesołowska, Anna; Pawłowski, Maciej; Newman-Tancredi, Adrian; Kolaczkowski, Marcin
[Journal of Medicinal Chemistry, 2020, vol. 63, # 19, p. 10946 - 10971]
[3]Sniecikowska, Joanna; Gluch-Lutwin, Monika; Bucki, Adam; Wiȩckowska, Anna; Siwek, Agata; Jastrzebska-Wiesek, Magdalena; Partyka, Anna; Wilczyńska, Daria; Pytka, Karolina; Latacz, Gniewomir; Przejczowska-Pomierny, Katarzyna; Wyska, Elżbieta; Wesołowska, Anna; Pawłowski, Maciej; Newman-Tancredi, Adrian; Kolaczkowski, Marcin
[Journal of Medicinal Chemistry, 2020, vol. 63, # 19, p. 10946 - 10971]