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CAS No. : | 701-54-2 | MDL No. : | MFCD00064951 |
Formula : | C8H15NO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | GYDJEQRTZSCIOI-UHFFFAOYSA-N |
M.W : | 157.21 | Pubchem ID : | 5526 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With barium(II) hydroxide In ethanol; lithium hydroxide monohydrate at 190℃; for 12h; | 13-14 Example 13: cis-trans isomer conversion step 200g of tranexamic acid cis-trans isomer mixture was added into the 3L reactor,Add barium hydroxide (3eq), pure water 1.2L, ethanol 400mL, heat to 190,The reaction was stopped for 12 hours, and when the temperature was lowered to room temperature, the pressure of the reactor was removed,The pH of the reaction solution was adjusted to 6.5-7.5 with sulfuric acid, and the barium sulfate solid was removed by suction filtration.The filtrate was concentrated to 1/3 of the original volume, cooled to 0 °C for crystallization, and dried by suction filtration.Trans-tranexamic acid was obtained with a purity of 99.1% (HPLC). |
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