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[ CAS No. 760-30-5 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
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Chemical Structure| 760-30-5
Chemical Structure| 760-30-5
Structure of 760-30-5 * Storage: {[proInfo.prStorage]}
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Product Details of [ 760-30-5 ]

CAS No. :760-30-5 MDL No. :MFCD18263132
Formula : C2H6N2OS Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 106.15 Pubchem ID :-
Synonyms :

Safety of [ 760-30-5 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P261-P264-P270-P271-P280-P285-P302+P352-P304+P340-P305+P351+P338-P310-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:2810
Hazard Statements:H301-H312-H315-H319-H332-H335-H334 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 760-30-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 760-30-5 ]

[ 760-30-5 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 623-51-8 ]
  • [ 760-30-5 ]
YieldReaction ConditionsOperation in experiment
91% With hydrazine hydrate In ethanol Reflux; 4.1.7. Mercapto-acetic acid hydrazide (7) To a solution of ethyl thioglycolate (11 mL, 0.10 mol, 1 equiv) in ethanol (30 mL) was added hydrazine monohydrate (5.8 mL, 0.12 mol, 1.2 equiv). The mixture was stirred at reflux overnight. The reaction progress was monitored by HPLC and, if necessary, small amounts of hydrazine (by portion of 0.2 equiv) were added until completion of the reaction. The reaction mixture was concentrated in vacuum yielding 9.65 mg (91%) of a yellow liquid corresponding to the expected acylhydrazine 7. 1H NMR (400 MHz, CDCl3) δ 7.75 (br s, 1H, NH), 3.90 (dd, 2H, NH2), 3.25 (s, 2H, CH2), 1.95 (t, 1H, SH). MS (EI): M+ m/z 106.0.
With methanol; hydrazine
With hydrazine hydrate
With hydrazine hydrate In ethanol Reflux;

  • 3
  • [ 34662-32-3 ]
  • [ 760-30-5 ]
  • 3-amino-6-chlorobenzo[b]thiophene-2-carbohydrazide [ No CAS ]
  • 4
  • [ 760-30-5 ]
  • [ 778-94-9 ]
  • 3-amino-6-(trifluoromethyl)benzo[b]thiophene-2-carbohydrazide [ No CAS ]
  • 5
  • [ 760-30-5 ]
  • [ 63-42-3 ]
  • D-lactose (2-sulfanylacetyl)hydrazone [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% In water; at 25℃; for 72h; General procedure: 2-Sulfanylacetohydrazide or 2-sulfanylbenzohydrazide, 11 mmol, was added to a solution of 3.60 g (10 mmol) of D-maltose or <strong>[63-42-3]D-<strong>[63-42-3]<strong>[63-42-3]lactose</strong> monohydrate</strong></strong> in 5 mL of hot water. The mixture was kept for 3 days at 25C, and the product was isolated by precipitation into acetone. The white crystalline solid was filtered off, dried under reduced pressure, and stored in a desiccator over P2O5. D-<strong>[63-42-3]Lactose</strong> (2-sulfanylacetyl)hydrazone (1a). Yield 3.02 g (70%), mp 171-173C (decomp.). 1H NMR spectrum (D2O), delta, ppm: A (55%): 3.51 br.s (1.10H, CH2S), 4.47 d (0.55H, 1-H, J= 7.5 Hz), 5.24 d (0.55H, 1'-H, J= 3.5 Hz); B(20%): 3.48 br.s (0.40H, CH2S), 5.24 d (0.20H, 1'-H, J= 3.5 Hz), 7.33 d (0.20H, HC=N, J= 3.5 Hz); C(25%), 3.32 d (0.25H, CH2S, JAB= 14.5 Hz), 3.40 d (0.25H, CH2S, JAB= 14.5 Hz), 4.68 d (0.25H, 1-H, J= 8.0 Hz), 5.24 d (0.25H, 1'-H, J= 3.5 Hz). 13C NMR spectrum (solid phase), deltaC, ppm: A(100%): 25.73 (CH2S), 62.64 (C6?, C6), 69.85 (C4?), 72.28 (C2?, C3?), 73.82 (C5, C5?), 76.32 (C2, C3), 83.09 (C4), 90.37 (C1), 104.56 (C1?), 176.40 (C=O). 13C NMR spectrum (D2O), deltaC, ppm: A: 23.98 (CH2S), 60.21 (C6, C6?), 69.67 (C4?), 72.25 (C2?, C3?), 74.78 (C5, C5?), 75.14 (C2), 75.64 (C3), 78.40 (C4), 89.18 (C1), 102.94 (C1?), 176.37 (C=O); B: 23.74 (CH2S), 60.92 (C6, C6?), 70.12 (C4?), 70.93 (C2?, C3?), 72.03 (C5, C5?), 72.97 (C2), 74.21 (C3), 78.55 (C4), 103.23 (C1?), 155.08 (C=N), 172.48 (C=O); C: 27.11 (CH2S), 61.09 (C6?), 62.09 (C6), 68.60 (C4?), 70.99 (C2?), 71.85 (C3?), 72.57 (C5, C5?), 72.70 (C2), 73.34 (C3), 73.56 (C1), 78.31 (C4), 102.94 (C1?), 176.50 (C=O). Found, %: C 39.14; H 6.03; N 6.60. C14H26N2O11S. Calculated, %: C 39.07; H 6.09; N 6.51.
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