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[ CAS No. 76684-89-4 ] {[proInfo.proName]}

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Chemical Structure| 76684-89-4
Chemical Structure| 76684-89-4
Structure of 76684-89-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 76684-89-4 ]

CAS No. :76684-89-4 MDL No. :MFCD00132882
Formula : C15H26N2O5 Boiling Point : -
Linear Structure Formula :- InChI Key :SCMSYZJDIQPSDI-SRVKXCTJSA-N
M.W : 314.38 Pubchem ID :123664
Synonyms :
Loxistatin acid;NSC 694279;EP 475

Safety of [ 76684-89-4 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 76684-89-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 76684-89-4 ]

[ 76684-89-4 ] Synthesis Path-Downstream   1~43

  • 1
  • [ 624-76-0 ]
  • [ 76684-89-4 ]
  • [ 140660-49-7 ]
YieldReaction ConditionsOperation in experiment
98% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 2
  • [ 115-20-8 ]
  • [ 76684-89-4 ]
  • [ 140676-34-2 ]
YieldReaction ConditionsOperation in experiment
91% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 3
  • [ 23032-21-5 ]
  • [ 76684-89-4 ]
  • [ 140660-57-7 ]
YieldReaction ConditionsOperation in experiment
89% With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 4
  • [ 371-62-0 ]
  • [ 76684-89-4 ]
  • [ 140660-46-4 ]
YieldReaction ConditionsOperation in experiment
75% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 5
  • [ 75-89-8 ]
  • [ 76684-89-4 ]
  • [ 140660-50-0 ]
YieldReaction ConditionsOperation in experiment
90% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 6
  • [ 75-80-9 ]
  • [ 76684-89-4 ]
  • [ 140660-51-1 ]
  • 7
  • [ 17849-38-6 ]
  • [ 76684-89-4 ]
  • [ 140660-52-2 ]
YieldReaction ConditionsOperation in experiment
96% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 8
  • [ 20776-45-8 ]
  • [ 76684-89-4 ]
  • [ 140660-60-2 ]
YieldReaction ConditionsOperation in experiment
88% With 4-methyl-morpholine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol In tetrahydrofuran at 0 - 20℃; for 25h;
  • 9
  • [ 21685-51-8 ]
  • [ 76684-89-4 ]
  • [ 140660-56-6 ]
YieldReaction ConditionsOperation in experiment
90% With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 10
  • [ 53157-48-5 ]
  • [ 76684-89-4 ]
  • [ 140660-54-4 ]
YieldReaction ConditionsOperation in experiment
With dmap; TEA; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride 1.) CH2Cl2, 0 deg C, 20 min, 2.) CH2Cl2, RT, 24 h; Yield given. Multistep reaction;
  • 11
  • [ 53157-50-9 ]
  • [ 76684-89-4 ]
  • [ 140660-55-5 ]
YieldReaction ConditionsOperation in experiment
With dmap; TEA; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride 1.) CH2Cl2, 0 deg C, 20 min, 2.) CH2Cl2, RT, 24 h; Yield given. Multistep reaction;
  • 13
  • [ 111507-07-4 ]
  • [ 76684-89-4 ]
  • [ 140849-90-7 ]
YieldReaction ConditionsOperation in experiment
78% With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 14
  • [ 117611-44-6 ]
  • [ 76684-89-4 ]
  • [ 140660-53-3 ]
YieldReaction ConditionsOperation in experiment
77% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 15
  • [ 76684-89-4 ]
  • [ 107-07-3 ]
  • [ 140660-47-5 ]
YieldReaction ConditionsOperation in experiment
80% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 16
  • [ 76684-89-4 ]
  • [ 540-51-2 ]
  • [ 140660-48-6 ]
YieldReaction ConditionsOperation in experiment
89% With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 3h;
  • 17
  • [ 2687-43-6 ]
  • [ 76684-89-4 ]
  • [ 179082-53-2 ]
YieldReaction ConditionsOperation in experiment
With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide 1.) DMF, 30 min, 2.) DMF, from 0 deg C to RT, 5 h; Yield given. Multistep reaction;
  • 18
  • [ 76684-89-4 ]
  • [ 543-27-1 ]
  • C20H34N2O7 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 4-methyl-morpholine In ethyl acetate; N,N-dimethyl-formamide at -20 - -15℃; for 0.166667h;
  • 19
  • [ 915697-62-0 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
53% With potassium hydroxide In ethanol at 0℃; for 0.5h;
  • 20
  • [ 915697-59-5 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 70 percent / MCPBA / CHCl3 / 50 °C 2: 53 percent / KOH / ethanol / 0.5 h / 0 °C
  • 21
  • [ 915697-61-9 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 76 percent / EDCI; HOBt; NMM / CH2Cl2 2: 70 percent / MCPBA / CHCl3 / 50 °C 3: 53 percent / KOH / ethanol / 0.5 h / 0 °C
  • 22
  • [ 915697-54-0 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 76 percent / LiOH; H2O / tetrahydrofuran; methanol / 0 °C 2: 76 percent / EDCI; HOBt; NMM / CH2Cl2 3: 70 percent / MCPBA / CHCl3 / 50 °C 4: 53 percent / KOH / ethanol / 0.5 h / 0 °C
  • 23
  • [ 107-85-7 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 76 percent / EDCI; HOBt; NMM / CH2Cl2 2: 70 percent / MCPBA / CHCl3 / 50 °C 3: 53 percent / KOH / ethanol / 0.5 h / 0 °C
Multi-step reaction with 4 steps 1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / ethyl acetate / 4 h / 3 - 20 °C 2: hydrogenchloride / ethyl acetate / 2.5 h / 20 °C 3: benzotriazol-1-ol; dicyclohexyl-carbodiimide / ethyl acetate / 15 h / 0 - 20 °C 4: potassium hydroxide / 5 h / Heating
  • 24
  • [ 13139-15-6 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 5 steps 1: N-methylmorpholine / ethyl acetate / 0.33 h 2: N-methylmorpholine / ethyl acetate 3: 100 percent / 4N HCl / dioxane / 0.75 h / Ambient temperature 4: N-methylmorpholine / ethyl acetate 5: 84 percent / 1N NaOH / ethanol / 1 h / 0 - 20 °C
Multi-step reaction with 4 steps 1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / ethyl acetate / 4 h / 3 - 20 °C 2: hydrogenchloride / ethyl acetate / 2.5 h / 20 °C 3: benzotriazol-1-ol; dicyclohexyl-carbodiimide / ethyl acetate / 15 h / 0 - 20 °C 4: potassium hydroxide / 5 h / Heating
  • 25
  • [ 66866-44-2 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: N-methylmorpholine / ethyl acetate 2: 100 percent / 4N HCl / dioxane / 0.75 h / Ambient temperature 3: N-methylmorpholine / ethyl acetate 4: 84 percent / 1N NaOH / ethanol / 1 h / 0 - 20 °C
  • 26
  • [ 84851-37-6 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: N-methylmorpholine / ethyl acetate 2: 84 percent / 1N NaOH / ethanol / 1 h / 0 - 20 °C
  • 27
  • [ 84863-67-2 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 100 percent / 4N HCl / dioxane / 0.75 h / Ambient temperature 2: N-methylmorpholine / ethyl acetate 3: 84 percent / 1N NaOH / ethanol / 1 h / 0 - 20 °C
Multi-step reaction with 3 steps 1: hydrogenchloride / ethyl acetate / 2.5 h / 20 °C 2: benzotriazol-1-ol; dicyclohexyl-carbodiimide / ethyl acetate / 15 h / 0 - 20 °C 3: potassium hydroxide / 5 h / Heating
  • 28
  • [ 76684-89-4 ]
  • (2S,3S)-3-Acetyl-oxirane-2-carboxylic acid [(S)-3-methyl-1-(3-methyl-butylcarbamoyl)-butyl]-amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: N-methylmorpholine / ethyl acetate; dimethylformamide / 0.17 h / -20 - -15 °C 2: ethyl acetate; dimethylformamide; diethyl ether / 0.5 h / Ambient temperature 3: 58 percent / aq. HI / CHCl3 / 0.5 h / 5 °C
  • 29
  • [ 76684-89-4 ]
  • (2S,3S)-Oxirane-2,3-dicarboxylic acid 2-hydroxyamide 3-[(S)-3-methyl-1-(3-methyl-butylcarbamoyl)-butyl]-amide} [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1.) HOBt, ethyl dimethylpropylamine carbodiimide, 2.) N-methylmorpholine / 1.) DMF, 30 min, 2.) DMF, from 0 deg C to RT, 5 h 2: 63 percent / H2 / 10percent Pd/C / methanol / 1 h
  • 30
  • [ 76684-89-4 ]
  • [ 179082-55-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: N-methylmorpholine / ethyl acetate; dimethylformamide / 0.17 h / -20 - -15 °C 2: ethyl acetate; dimethylformamide; diethyl ether / 0.5 h / Ambient temperature
  • 31
  • [ 76684-89-4 ]
  • [ 140660-58-8 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 88 percent / HOBT, N-methylmorpholine, BOP-Cl / tetrahydrofuran / 25 h / 0 - 20 °C 2: 96 percent / H2 / 10percent Pd/C / ethanol / 4 h
YieldReaction ConditionsOperation in experiment
With cruzain In dimethyl sulfoxide at 25℃; for 0.0833333h;
  • 33
  • [ 84851-37-6 ]
  • [ 76684-89-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / ethyl acetate / 15 h / 0 - 20 °C 2: potassium hydroxide / 5 h / Heating
  • 34
  • [ 955370-01-1 ]
  • [ 76684-89-4 ]
  • C22H40N4O6 [ No CAS ]
  • 35
  • [ 76684-89-4 ]
  • [ 737001-67-1 ]
  • C23H42N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h;
  • 36
  • [ 457897-22-2 ]
  • [ 76684-89-4 ]
  • C24H44N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h;
  • 37
  • [ 1451983-25-7 ]
  • [ 76684-89-4 ]
  • C25H46N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h;
  • 38
  • [ 76684-89-4 ]
  • [ 259870-73-0 ]
  • C26H48N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h;
  • 39
  • [ 76684-89-4 ]
  • [ 175233-53-1 ]
  • C23H42N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h;
  • 40
  • [ 76684-89-4 ]
  • 1-(2-methylpropyl)hydrazinecarboxylic acid tert-butyl ester [ No CAS ]
  • C24H44N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h;
  • 41
  • [ 76684-89-4 ]
  • hydrazinecarboxylic acid tert-butyl ester hydrochloride [ No CAS ]
  • C20H36N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 3h;
  • 42
  • [ 21075-83-2 ]
  • [ 76684-89-4 ]
  • C21H38N4O6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3h;
  • 43
  • [ 76684-89-4 ]
  • [ 1451982-40-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 3 h / 20 °C 2: trifluoroacetic acid / water / 0.5 h / 20 °C
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