Select Region or Location
Americas
  • Argentina
  • Brazil
  • Canada
  • Mexico
  • United States
  • Other Americas
Europe
  • Austria
  • Belgium
  • Bulgaria
  • Croatia/Hrvatska
  • Cyprus
  • Czech Republic
  • Denmark
  • Estonia
  • Finland
  • France
  • Germany
  • Greece
  • Hungary
  • Ireland
  • Italy
  • Latvia
  • Liechtenstein
  • Lithuania
  • Luxembourg
  • Malta
  • Netherlands
  • Norway
  • Poland
  • Portugal
  • Romania
  • Slovak Republic
  • Slovenia
  • Spain
  • Sweden
  • Switzerland
  • Turkey
  • United Kingdom
  • Other Europe
Asia Pacific
  • Australia
  • China
  • India
  • Indonesia
  • Japan
  • Korea, Republic of
  • Malaysia
  • New Zealand
  • Philippines
  • Singapore
  • Thailand
  • Vietnam
  • Other Asia Pacific
Africa And Middle East
  • Egypt
  • Israel
  • Other Africa And Middle East
USD
Home Cart Sign in  
Chemical Structure| 798564-92-8 Chemical Structure| 798564-92-8

Structure of 798564-92-8

Chemical Structure| 798564-92-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only! Not for Human Use. We Do Not Sell to Patients.

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

DE Stock

US Stock

Asia Stock

Global Stock

In Stock
{[ item.pr_size ]}{[ size_append_text(item.pr_size, proInfo.prAm, 'list') ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

  • {[ item.pr_size ]}
    {[ size_append_text(item.pr_size, proInfo.prAm, 'list') ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 798564-92-8 ]

CAS No. :798564-92-8
Formula : C10H10F2O2
M.W : 200.18
SMILES Code : O=CC1=C(F)C=CC(OC(C)C)=C1F
English Name :2,6-Difluoro-3-isopropoxybenzaldehyde
MDL No. :MFCD18824342

Safety of [ 798564-92-8 ]

Application In Synthesis of [ 798564-92-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 798564-92-8 ]

[ 798564-92-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 203059-83-0 ]
  • [ 68-12-2 ]
  • [ 798564-92-8 ]
YieldReaction ConditionsOperation in experiment
Stage #1: 1,3-difluoro-4-isopropoxybenzene With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78 - -75℃; for 0.5h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; cyclohexane at -40 - 0℃; for 0.666667h; 56 Example 56; 1- (2, 6-DIFLUORO-3-ISOPROPOXY-BENZOYL)-6, 7-DIMETHOXY-ISOQUINOLINE-4-CARBOXYLIC ACID ; compound with TRIFLUORO-ACETIC acid 22 g (140 mmol) of 1, 3- difluoro-4-isopropoxybenzene was dissolved in 175 ML of freshly distilled THF and the stirring mixture chilled to-78°C under argon. 165 mL of 1.3 M sec-butyl lithium solution in cyclohexane (215 mmol) was added slowly (over 20 minutes) by cannula under argon pressure. When addition was complete the mixture was stirred at-75 °C for 10 minutes. A solution of DMF (19 ML : 245 mmol) and THF (25 ML) was added to the stirring mixture all at once. Temperature rose to-40°C then subsided. The mixture was then stirred at 0°C for 40 minutes. The mixture was 200 ML of hexanes and stirred with 200 mL of saturated aqueous ammonium chloride. Phases were separated; the organic phase was washed with brine; the aqueous phase was extracted further with 200 ML of ethyl ether. Organic solutions were combined, dried (magnesium sulfate), filtered and evaporated to give 24 g of the crude aldehyde which was purified by silica gel chromatography, eluting with gradient mixtures of ethyl acetate and hexanes. The process yielded 14.6 g of purified aldehyde as a pale green oil.
 

Historical Records

Technical Information

Categories