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[ CAS No. 84227-70-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 84227-70-3
Chemical Structure| 84227-70-3
Structure of 84227-70-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 84227-70-3 ]

CAS No. :84227-70-3 MDL No. :MFCD07343995
Formula : C12H20N2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 192.30 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 84227-70-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 84227-70-3 ]

[ 84227-70-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 69293-74-9 ]
  • [ 84227-70-3 ]
YieldReaction ConditionsOperation in experiment
67% With lithium aluminium tetrahydride In diethyl ether at 0 - 20℃; for 12h; Inert atmosphere; o-(Diethylaminomethyl)benzylamine (6) General procedure: o-(Diethylaminomethyl)benzonitrile (13) (6.0 g, 32 mmol) in anhydrous diethylether (20 mL) was added dropwiseover a period of 10 min to a suspension of LiAlH4 (2.4 g, 64 mmol) in anhydrous diethylether (50 mL, 0°C, N2 atmosphere). The mixture was allowed to come to room temperature,stirred for 12 h, cooled in ice, treated dropwise with 20% NaOH (17 mL) with cooling, andextracted three times with ether (50 mL each). The combined organic phases were dried overNa2SO4, filtered, and evaporated under vacuum. The product was collected as reddish-orangecolored oil.
With tetralin; nickel at 70℃; Hydrogenation;
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