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[ CAS No. 85630-84-8 ] {[proInfo.proName]}

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Chemical Structure| 85630-84-8
Chemical Structure| 85630-84-8
Structure of 85630-84-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 85630-84-8 ]

CAS No. :85630-84-8 MDL No. :MFCD11940800
Formula : C8H5Cl3O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 239.48 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 85630-84-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 85630-84-8 ]

[ 85630-84-8 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 364-62-5 ]
  • [ 85630-84-8 ]
  • [ 85630-58-6 ]
YieldReaction ConditionsOperation in experiment
59.7% With triethylamine In toluene for 6h; Heating;
  • 2
  • [ 2976-74-1 ]
  • [ 85630-84-8 ]
YieldReaction ConditionsOperation in experiment
With thionyl chloride; for 5h;Reflux; General procedure: Substituted benzoyl and phenoxyacetyl chlorides 12a-c and 16a-e were obtained by refluxing for 5 h the appropriate acid derivatives (0.01 mol) with thionyl chloride (7.25 mL). After evaporation under reduced pressure, the crude liquid residue was used for subsequent reactions without purification.
With phosphorus pentachloride; In dichloromethane;Reflux; General procedure: To a solution of phosphorus pentachloride (0.126 g, 0.610 mmol) in dichloromethane (11 mL), phenoxyacetic acid (0.092 g, 0.610 mmol) was added with stirring and the mixture refluxed for 30-40 minutes. After cooling, 4-methyl-1,2,5-oxadiazol-3-amine (0.060 g, 0.610 mmol) was added and the solution refluxed for 2-2.5 hours. The solvent was removed under reduced pressure and the residue quenched with water (50 mL). The solid was collected by vacuum filtration and washed with saturated sodium bicarbonate solution followed by water to afford compound 19 (0.103 g, 73%)
  • 3
  • [ 85630-84-8 ]
  • [ 25900-61-2 ]
  • N-(3-methylcarbamoylphenyl)-2,3-dichlorophenoxyacetamide [ No CAS ]
  • 4
  • [ 5004-88-6 ]
  • [ 85630-84-8 ]
  • 2-(2-(2,3-dichlorophenoxy)acetamido)-4,5-dimethoxybenzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
15% With pyridine; at 0 - 5℃; for 24.5h; General procedure: To a cold (0-5 C) stirred suspension of aminobenzamides 15a-f and 20a,b (0.016 mol) in pyridine (13 mL), 0.016 mol of the appropriate phenoxyacetyl chloride 16a-e was added over 30 min. After addition was complete, the solution was stirred for24 h and then poured onto crushed ice. The precipitate was removed by filtration, washed with water, and crystallized from the indicated solvent.
  • 5
  • [ 17647-70-0 ]
  • [ 85630-84-8 ]
  • 2-(2,3-dichlorophenoxy)-N-(4-methyl-1,2,5-oxadiazol-3-yl)acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.179 g In dichloromethane Reflux; General procedure: To a solution of phosphorus pentachloride (0.126 g, 0.610 mmol) in dichloromethane (11 mL), phenoxyacetic acid (0.092 g, 0.610 mmol) was added with stirring and the mixture refluxed for 30-40 minutes. After cooling, 4-methyl-1,2,5-oxadiazol-3-amine (0.060 g, 0.610 mmol) was added and the solution refluxed for 2-2.5 hours. The solvent was removed under reduced pressure and the residue quenched with water (50 mL). The solid was collected by vacuum filtration and washed with saturated sodium bicarbonate solution followed by water to afford compound 19 (0.103 g, 73%)
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