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[ CAS No. 91004-40-9 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 91004-40-9
Chemical Structure| 91004-40-9
Structure of 91004-40-9 *Storage: {[proInfo.prStorage]}

Quality Control of [ 91004-40-9 ]

Purity: {[proInfo.showProBatch.pb_purity]}

Related Doc. of [ 91004-40-9 ]

SDS

Product Details of [ 91004-40-9 ]

CAS No. :91004-40-9MDL No. :
Formula :C9H9NO4Boiling Point :-
Linear Structure Formula :-InChI Key :-
M.W :195.17Pubchem ID :-
Synonyms :

Computed Properties of [ 91004-40-9 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 91004-40-9 ]

Signal Word:Class
Precautionary Statements:UN#:
Hazard Statements:Packing Group:

Application In Synthesis of [ 91004-40-9 ]

  • Downstream synthetic route of [ 91004-40-9 ]

[ 91004-40-9 ] Synthesis Path-Downstream   1~3

  • 2
  • [ 91004-40-9 ]
  • [ 100-46-9 ]
  • [ 142071-84-9 ]
  • 3
  • [ 5781-53-3 ]
  • [ 95-55-6 ]
  • [ 91004-40-9 ]
YieldReaction ConditionsOperation in experiment
1.2 g With triethylamine; In N,N-dimethyl-formamide; for 0.166667h;Cooling with ice; A mixture of 2.25 g of methyl chloroglyoxylate and5 ml of DMF was added dropwise to a mixture of 2.0 g of2-aminophenol, 2.23 g of triethylamine, and 20 ml of DMF under ice cooling, followed by stirring for 10 minutes. Water and 1 M hydrochloric acid were added thereto, and the precipitated solids were collected by filtration. The obtained solids were washed with water and dried under reduced pressure, thereby obtaining 1.2 g of methyl 2-[(2-hydroxyphenyl) amino] -2-oxo-acetate.11217] ?H-NMR (DMSO-D5) oe: 10.24 (s, 1H), 9.62 (br s,1H), 7.95-7.92 (m, 1H), 7.05-7.00 (m, 1H), 6.94-6.90 (m,1H), 6.86-6.80 (m, 1H), 3.85 (s, 3H)
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