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[ CAS No. 91658-91-2 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 91658-91-2
Chemical Structure| 91658-91-2
Chemical Structure| 91658-91-2
Structure of 91658-91-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 91658-91-2 ]

CAS No. :91658-91-2 MDL No. :MFCD10566792
Formula : C7H5BrO3 Boiling Point : -
Linear Structure Formula :- InChI Key :GBPZLKQDSNPABG-UHFFFAOYSA-N
M.W : 217.02 Pubchem ID :57474212
Synonyms :

Safety of [ 91658-91-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 91658-91-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 91658-91-2 ]

[ 91658-91-2 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 91658-91-2 ]
  • [ 166383-81-9 ]
  • (2S,4S)-1-[(2S,3S)-3-(2-Bromo-3-hydroxy-benzoylamino)-2-hydroxy-4-phenyl-butyryl]-4-chloro-pyrrolidine-2-carboxylic acid tert-butylamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran for 24h; Ambient temperature; Yield given;
YieldReaction ConditionsOperation in experiment
With copper(I) bromide
  • 3
  • (4-(but-3-en-1-yl)-2-methoxy-6-methylpyridin-3-yl)methanamine [ No CAS ]
  • [ 91658-91-2 ]
  • 2-bromo-N-((4-(but-3-en-1-yl)-2-methoxy-6-methylpyridin-3-yl)methyl)-3-hydroxybenzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
69.6% With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride at 20℃; 84.a (a) 2-bromo-N-((4-(but-3-en-l-yl)-2-methoxy-6-methylpyridin-3-yl)methyl)-3- hydroxybenzamide (a) 2-bromo-N-((4-(but-3-en-l-yl)-2-methoxy-6-methylpyridin-3-yl)methyl)-3- hydroxybenzamide A mixture of 2-bromo-3-hydroxybenzoic acid (1 g, 4.61 mmol), (4-(but-3-en-l-yl)- 2-methoxy-6-methylpyridin-3-yl)methanamine (1.141 g, 5.53 mmol), HO At (0.941 g, 6.91 mmol), EDC (1.325 g, 6.91 mmol), and N-methylmorpholine (1.520 mL, 13.82 mmol) was stirred at room temperature over the weekend. The reaction mixture was poured into water and stirred for 1 h. The precipitate was collected by filtration, and dried at the pump overnight. The residue was dissolved in EtOAc (200 mL) and washed with water (30 mL), then brine (30 mL), then the organic layer was dried over Na2S04, filtered, cand oncentrated to afford an orange solid. The solid was purified by flash column chromatography (0-50% EtOAc in hexanes, 40 g column) to afford 2-bromo-N-((4-(but-3- en-l-yl)-2-methoxy-6-methylpyridin-3-yl)methyl)-3-hydroxybenzamide (1.3 g, 3.21 mmol, 69.6 % yield) as a pale orange oil. LC-MS(ES) m/z = 405.2, 407.2 [M+H]+.
  • 4
  • [ 91658-91-2 ]
  • [ 99-06-9 ]
YieldReaction ConditionsOperation in experiment
85% With sodium sulfite In water at 130℃; for 3h; Sealed tube; Microwave irradiation; Green chemistry;
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