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[ CAS No. 916602-09-0 ]

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Chemical Structure| 916602-09-0
Chemical Structure| 916602-09-0
Structure of 916602-09-0 * Storage: {[proInfo.prStorage]}

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Product Details of [ 916602-09-0 ]

CAS No. :916602-09-0 MDL No. :MFCD12910960
Formula : C9H11ClFNO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :219.64 g/mol Pubchem ID :-
Synonyms :

Safety of [ 916602-09-0 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 916602-09-0 ]

  • Downstream synthetic route of [ 916602-09-0 ]

[ 916602-09-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 19883-57-9 ]
  • [ 916602-09-0 ]
YieldReaction ConditionsOperation in experiment
100% With thionyl chloride; at 0 - 75℃; for 2h; General procedure: The methyl-esterification reaction of L-phenylalanine.To a suspension of L-phenylalanine (1 g, 6.05 mmol, 1.0 equiv) inmethanol (25 mL) cooled to 0 C was added thionyl chloride(475 mL, 6.66 mmol, 1.5 equiv) slowly. After 10 min, the reactionmixture was heated to 75 C to reflux for 2 h. After completion(monitored by TLC), the solvent was removed in vacuo, and at thistime, a white solid was formed methyl L-phenylalaninate hydrochloride(1.23 g, quantitative yield).
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