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[ CAS No. 916791-27-0 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 916791-27-0
Chemical Structure| 916791-27-0
Structure of 916791-27-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 916791-27-0 ]

CAS No. :916791-27-0 MDL No. :MFCD08752706
Formula : C8H6BrNO4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 260.04 Pubchem ID :-
Synonyms :

Safety of [ 916791-27-0 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3261
Hazard Statements:H302-H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 916791-27-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 916791-27-0 ]

[ 916791-27-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3113-71-1 ]
  • [ 916791-27-0 ]
YieldReaction ConditionsOperation in experiment
68% With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In benzene for 12h; Reflux; Sealed tube; [003061 A solution of 3-methyl-4-nitrobenzoic acid (539 mg, 2.98 mmol) in benzene (20 mL) was heated to reflux in a sealed tube after which N-bromosuccinimide (679 mg, 3.43 mol) and AIBN (49 mg, 0.298 mol) were carefully added in a portion wise manner over 5 mm. After 12 h the mixture was cooled to room temperature, and the succinimide was filtered off and washed with benzene (5 mL x 3). The solvent was removed under reduced pressure and purified by column chromatography to give the desired product 3-(bromomethyl)-4- nitrobenzoic acid (553 mg, 68% yield) as a viscous yellow oil.
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