Alternatived Products of [ 935-12-6 ]
Alternatived Products of [ 935-12-6 ]
Product Details of [ 935-12-6 ]
CAS No. : | 935-12-6 | MDL No. : | MFCD03412485 |
Formula : |
C7H12O3
|
Boiling Point : |
263°C at 760 mmHg |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 144.17 | Pubchem ID : | - |
Synonyms : |
|
Computed Properties of [ 935-12-6 ]
TPSA :Topological Polar Surface Area |
- |
H-Bond Acceptor Count : |
- |
XLogP3 : |
- |
H-Bond Donor Count : |
- |
SP3 : |
- |
Rotatable Bond Count : |
- |
Safety of [ 935-12-6 ]
Signal Word: | | Class: | |
Precautionary Statements: | | UN#: | |
Hazard Statements: | | Packing Group: | |
Application In Synthesis of [ 935-12-6 ]
- Downstream synthetic route of [ 935-12-6 ]
- 1
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[ 935-13-7 ]

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[ 935-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
|
With hydrogen; palladium; In methanol; at 60℃; under 22502.3 Torr; |
A mixture of 3-(furan-2-yl)propanoic acid (11.0 g, 80.0 mmol) and Pd/C (1.1 g, 10%) in MeOH (110 mL) was stirred at 60 C under 30 bar of H2 overnight. The mixture was then filtered and the filtrate was concentrated in vacuo to give the title compound, which was used for next step without further purification. |
|
With palladium on activated charcoal; hydrogen; In methanol; at 60℃; under 22502.3 Torr; |
A mixture of 3-(furan-2-yl)propanoic acid (11.0 g, 80.0 mmol) and Pd/C (1.1 g, 10%) in MeOH (110 mL) was stirred at 60 C. under 30 bar of H2 overnight. The mixture was then filtered and the filtrate was concentrated in vacuo to give the title compound, which was used for next step without further purification. |
Reference:
[1]Zhurnal Obshchei Khimii,1938,vol. 8,p. 7,14
Chemisches Zentralblatt,1939,vol. 110,p. 1969
[2]Patent: WO2014/12360,2014,A1 .Location in patent: Paragraph 00442
[3]Patent: US2015/87639,2015,A1 .Location in patent: Paragraph 0768