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CAS No. : | 942195-55-3 | MDL No. : | MFCD30533430 |
Formula : | C20H19F2N3O3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 387.38 | Pubchem ID : | - |
Synonyms : |
CJ-12420;RQ-00000004;LXI-15028;K-CAB;IN-A001
|
Chemical Name : | (S)-7-((5,7-Difluorochroman-4-yl)oxy)-N,N,2-trimethyl-1H-benzo[d]imidazole-5-carboxamide |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330 | UN#: | |
Hazard Statements: | H302-H315-H319 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / Inert atmosphere; Cooling with ice 2.1: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran; water / 3 h / 1292.9 Torr 3.1: sodium acetate / dichloromethane / 1 h 4.1: N-chloro-succinimide / acetonitrile / 0.58 h / 5 °C 4.2: 2 h / 20 °C | ||
Multi-step reaction with 4 steps 1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / Inert atmosphere; Cooling with ice 2.1: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran; water / 3 h / 1292.9 Torr 3.1: sodium acetate / dichloromethane / 24 h / 20 °C 4.1: N-chloro-succinimide / acetonitrile / 0.58 h / 5 °C 4.2: 2 h / 20 °C |