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[ CAS No. 960041-69-4 ] {[proInfo.proName]}

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Chemical Structure| 960041-69-4
Chemical Structure| 960041-69-4
Structure of 960041-69-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 960041-69-4 ]

CAS No. :960041-69-4 MDL No. :
Formula : C18H16N6 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 316.36 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 960041-69-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 960041-69-4 ]

[ 960041-69-4 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 288-88-0 ]
  • [ 1667-10-3 ]
  • [ 960041-69-4 ]
YieldReaction ConditionsOperation in experiment
54% With potassium carbonate; potassium iodide; In acetone; for 10.5h;Reflux; the ligandBBPTZ was prepared according to the literature [12]. 1,2,4-triazole (1.38 g,20 mmol) was dissolved in acetone (30 mL), and then PEG-400 (2 g), anhydrouspotassium carbonate (5 g), and potassium iodide (0.5 g) were added to the abovesolution. After the solution was stirring for 30 min, <strong>[1667-10-3]4,4'-bis(chloromethyl)biphenyl</strong>(2.5 g, 10 mmol) was added. The mixture was vigorously stirred and refluxed for10 h. A white residue was obtained after filtering and distilling off the filtrate. Thecrude product was re-crystallized from hot water to give white crystalline product.Yield: 1.7 g (54%). Anal. Calcd for C18H16N6: C, 68.34; H, 5.10; N, 26.56. Found: C,68.26; H, 5.02; N, 25.50. IR (KBr)/cm-1: 3099(w), 1508s (s), 1269 (s), 1140 (s),1014 (s) 751(s).
  • 2
  • [ 960041-69-4 ]
  • [ 7717-76-2 ]
  • [ 7732-18-5 ]
  • [ 6046-93-1 ]
  • ([Cu(H2odpa)(4,4'-bis[(1,2,4-triazol-1-yl)methyl]biphenyl)(H2O)]*2H2O)n [ No CAS ]
  • 3
  • [ 960041-69-4 ]
  • α-H4SiMo12O40*xH2O [ No CAS ]
  • [ 6018-89-9 ]
  • 5C18H16N6*2Ni(2+)*8H2O*Mo12O40Si(4-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% Stage #1: 4,4′-bis((1H-1,2,4-triazol-1-yl)methyl)biphenyl; α-H4SiMo12O40*xH2O; nickel(II) acetate tetrahydrate In water at 20℃; for 0.5h; Stage #2: With hydrogenchloride In water at 140℃; for 72h; Sealed tube; Autoclave; High pressure; [Ni2(H2O)2(BBPTZ)5][SiMo12O40]·6H2O A mixture of H4SiMo12O40·nH2O[12] (0.153 g, 0.075 mmol), Ni(OAc)2·4H2O (0.0475 g, 0.25 mmol) and BBPTZ[13] (0.1 g, 0.32 mmol) was dissolved in 10 mL of distilled water at room temperatureand stirred for 0.5 h. The pH of the reaction mixture was adjusted to about 3.0 with 1.0 M HCl. The suspension was sealed in a 23-mL Teflon-lined autoclave andheated at 140 °C for 3 days. After slow cooling to room temperature, green blockcrystals were filtered and washed with distilled water (60% yield based on Mo).Anal. Calcd for C90H96N30O48SiMo12Ni2: C, 29.48; H, 2.62; N, 11.47; Mo, 31.45; Ni,3.20. Found: C, 29.69; H, 2.87; N, 11.25; Mo, 31.23; Ni, 3.35. Selected IR (KBr pellet,cm-1): 3421(m), 3115(m), 1516(s), 1425(m), 1281(m), 1209(m), 1128(s), 1063(s), 962(s), 872(w), 800(s). TG analysis shows that the first weight loss of 4.02%in the temperature range of 75-140 °C corresponds to six lattice water moleculesand two coordinated water molecules in 2 (calculated value 3.93%). Phase puritywas confirmed by the powder X-ray diffraction (Fig. S18 and Fig. S19).
  • 4
  • [ 960041-69-4 ]
  • [ 13799-90-1 ]
  • [ 7732-18-5 ]
  • [ 563-63-3 ]
  • [silver(I)(4,4'-bis(1,2,4-triazol-1-ylmethyl)biphenyl)(2,5-dichloroterephthalic acid)]*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
32% at 140℃; for 3h;Autoclave; High pressure; General procedure: A mixture of AgOAc (0.2 mmol, 33.4 mg), L (0.1 mmol,31.6 mg), H2mip (0.1 mmol, 17.8 mg), and H2O (10 mL) was sealed in a 25 mL Teflon-lined autoclave and heated to 140 C for 3 days under autogenous pressure. Afterward, the autoclave was cooled to room temperature at a rate of 5 C h-1
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