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Chemical Structure| 962-07-2 Chemical Structure| 962-07-2

Structure of 962-07-2

Chemical Structure| 962-07-2

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Product Details of [ 962-07-2 ]

CAS No. :962-07-2
Formula : C16H15NO2
M.W : 253.30
SMILES Code : O=C(NC1=CC=C(C)C=C1)CC(C2=CC=CC=C2)=O
English Name :3-Oxo-3-phenyl-N-(p-tolyl)propanamide

Safety of [ 962-07-2 ]

Application In Synthesis of [ 962-07-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 962-07-2 ]

[ 962-07-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50743-18-5 ]
  • [ 962-07-2 ]
  • [ 1645301-19-4 ]
YieldReaction ConditionsOperation in experiment
61% With 1,8-diazabicyclo[5.4.0]undec-7-ene In ethanol for 0.5h; Reflux; 7-Methyl-N-(4-methylphenyl)-5-oxo-2-phenyl-5H-chromeno[2,3-b]pyridine-3-carboxamide (19) B. A mixture of nitrile 1 (0.55 g, 3.0 mmol) and N-(4-methylphenyl)-3-oxo-3-phenylpropanamide (0.76 g, 3.0 mmol) in abs. EtOH (20 ml) containing DBU (0.1 ml, 0.7 mmol) was refluxed for 30 min. The pale-yellow crystals obtained during heating were filtered off and recrystallized from DMF-MeOH. Yield 0.77 g (61%), white crystals, mp 309-310°C.
 

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