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CAS No. : | 99-68-3 | MDL No. : | MFCD00002720 |
Formula : | C6H8O6S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | JPHVSDWIWBDHOC-UHFFFAOYSA-N |
M.W : | 208.19 | Pubchem ID : | 97922 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
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With sulfuric acid; benzene unter Entfernen des entstehenden Wassers; |
Yield | Reaction Conditions | Operation in experiment |
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With toluene in Gegenwart eines sauren Katalysators; | ||
With benzene in Gegenwart eines sauren Katalysators; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium hydrogen sulfate; benzene unter Entfernen des entstehenden Wassers; |
Yield | Reaction Conditions | Operation in experiment |
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With sodium hydrogen sulfate; benzene unter Entfernen des entstehenden Wassers; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium hydrogen sulfate; benzene unter Entfernen des entstehenden Wassers; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogenchloride |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
at 70℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With water |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With alkali levorotatory form; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With toluene in Gegenwart eines sauren Katalysators; | ||
With benzene in Gegenwart eines sauren Katalysators; | ||
With hydrogenchloride In water at 90℃; for 2h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium hydrogen sulfate; benzene unter Entfernen des entstehenden Wassers; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
(hydrolysis); |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
(i) KOH, EtOH, (ii) aq. H2SO4, Et2O; Multistep reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In water examination of further solvents; electrolysis; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
at 90℃; Geschwindigkeit der Racemisierung; levorotatory form; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
at 90℃; Geschwindigkeit der Racemisierung; levorotatory form; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
at 90℃; Geschwindigkeit der Racemisierung; levorotatory form; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium hydroxide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In water pH=1 to 6; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With Ni salt; H2O In water pH:3-10; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium hydroxide In water at 90℃; for 48h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With thionyl chloride In N,N-dimethyl-formamide at 20 - 150℃; Schlenk technique; Inert atmosphere; | 1.d (d) Synthesis of2-(2-chloro-2-oxo-ethyl)sulfanylbutanedioyl dichloride (Acyl Chloride 4) In a Schlenk tube, previously dried in an oven at 150°C, SOCh (10.0 mL, 138 mmol) and 3 drops of DMF were added to 2-(carboxymethylsulfanyl)butanedioic acid (4.30 g, 20 mmol, origin: Alfa Aesar). The reaction mixture was stirred at room temperature over the week-end under a flow of nitrogen, which was neutralised through a wash bottle containing an aqueous solution of NaOH (10%). An aliquot of the reaction mixture (0.1 mL) was pipetted off and placed in a small vial. After evaporating the SOCI2 and flushing with argon, the sample (38 mg) was analyzed by NMR spectroscopy. The SOCI2 of the rest of the sample was evaporated and flushed with argon to afford the target compound. ^-NMR: 4.43 (d, J = 17.3 Hz, 1 H); 4.31-4.24 (m, 1 H), 4.21 (d, J = 17.3 Hz, 1 H), 3.44 (dd, J = 18.9, 9.9 Hz, 1 H), 2.94-2.79 (m, 1 H). 13C-NMR: 171.65, 170.49, 169.21, 45.20, 40.64, 35.75. |
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