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[ CAS No. 99548-57-9 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 99548-57-9
Chemical Structure| 99548-57-9
Structure of 99548-57-9 *Storage: {[proInfo.prStorage]}

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Product Details of [ 99548-57-9 ]

CAS No. :99548-57-9MDL No. :MFCD01846086
Formula : C9H9BrO3 Boiling Point : -
Linear Structure Formula :-InChI Key :N/A
M.W :245.07Pubchem ID :-
Synonyms :

Computed Properties of [ 99548-57-9 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 99548-57-9 ]

Signal Word:WarningClass:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 99548-57-9 ]

  • Downstream synthetic route of [ 99548-57-9 ]

[ 99548-57-9 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 97-53-0 ]
  • [ 99548-57-9 ]
YieldReaction ConditionsOperation in experiment
With phosphorus tribromide at 120℃; Behandeln des Reaktionsprodukts mit wss. KMnO4;
  • 2
  • [ 203805-64-5 ]
  • [ 99548-57-9 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide In ethanol at 60℃; for 0.166667h;
  • 3
  • [ 99548-57-9 ]
  • C9H8BrClO2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 3h; 24.A Step A: 6-Bromo-7-methoxy-3,4-dihydronaphthalen-2(lH -one Step A: 6-Bromo-7-methoxy-3,4-dihydronaphthalen-2(lH -one:To a DCM solution of (4-Bromo-3-methoxyphenyl)acetic acid (900 mg, 3.67 mmol) was added oxalyl chloride (0.64 ml, 7.3 mmol) and a drop of DMF. The solution was allowed to stir at RT for 3 hours, at which point bubbling stopped. The volatiles were removed under vacuum, and the residue was redissolved in DCM. The solution was cooled to 0 °C. To this solution was added aluminum trichloride (1.2 g, 9.2 mmol). After stirring the mixture for 15 minutes, ethylene was bubbled into the reaction. The reaction was poured into ice, extracted with DCM, washed with brine, and purified by MPLC. LC-MS (IE, m/z) 255 [M + 1]+.
  • 4
  • [ 99548-57-9 ]
  • [ 1336948-57-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C 2: aluminum (III) chloride / dichloromethane / 0.25 h / 0 °C
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