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Chemical Structure| 34404-36-9 Chemical Structure| 34404-36-9
Chemical Structure| 34404-36-9

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Product Details of Boc-Lys(Z)-OSu

CAS No. :34404-36-9
Formula : C23H31N3O8
M.W : 477.51
SMILES Code : O=C(ON1C(CCC1=O)=O)[C@@H](NC(OC(C)(C)C)=O)CCCCNC(OCC2=CC=CC=C2)=O
MDL No. :MFCD00037915

Safety of Boc-Lys(Z)-OSu

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of Boc-Lys(Z)-OSu

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34404-36-9 ]

[ 34404-36-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 34404-36-9 ]
  • [ 22802-67-1 ]
  • [ 1294448-57-9 ]
YieldReaction ConditionsOperation in experiment
98% In chloroform; at 20℃; for 60h;Inert atmosphere; A mixture of 47.75 g (100.0 mmol) of 1 and 18.12 g (100.0 mmol) of 2 in 500 mL of anhydrous CHCl3 was stirred at room temperature under Ar and, after 30 minutes, a clear orange solution was observed. The reaction was monitored by tlc and found to be complete after 60 hours. The reaction was concentrated in vacuo to a brown syrup that was dissolved between EtOAc and water. The layers were separated and the aqueous layer was extracted twice more with EtOAc. The EtOAc fractions were combined and washed four times with water (followed removal of byproduct HOSu by tlc). The EtOAc layer was then washed once with 10% citric acid (aqueous), twice with water, three times (carefully) with saturated NaHCO3, and once with brine. The EtOAc layer was dried over Na2SO4, filtered, and concentrated to afford 53.48 g (98%) of 3.
 

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