Home Cart Sign in  
Chemical Structure| 7292-71-9 Chemical Structure| 7292-71-9
Chemical Structure| 7292-71-9

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

Synonyms: 2-Amino-2-(3-chlorophenyl)acetic acid

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of H-DL-Phg(3-Cl)-OH

CAS No. :7292-71-9
Formula : C8H8ClNO2
M.W : 185.61
SMILES Code : O=C(O)C(N)C1=CC=CC(Cl)=C1
Synonyms :
2-Amino-2-(3-chlorophenyl)acetic acid
MDL No. :MFCD00049326
InChI Key :MGOUENCSVMAGSE-UHFFFAOYSA-N
Pubchem ID :290730

Safety of H-DL-Phg(3-Cl)-OH

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of H-DL-Phg(3-Cl)-OH

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7292-71-9 ]

[ 7292-71-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 7292-71-9 ]
  • [ 179811-63-3 ]
YieldReaction ConditionsOperation in experiment
100% a) (RS)-2-Amino-2-(3-chloro-phenyl)-ethanolTo a stirred solution of lithium borohydride in THF (10.5 ml, 2 M solution) under an argon atmosphere was added dropwise chlorotrimethylsilane (5.34 ml). The resulting suspension was cooled to 0 0C and amino-(3-chlorophenyl)-acetic acid (2.0 g) was added portionwise. The ice bath was removed and stirring at r.t. was then continued for 16 h. The mixture was quenched by dropwise addition of methanol (15 ml) and then concentrated in vacuo. The residue was suspended in ethyl acetate and washed with 2 N aq NaOH. The phases were separated and the aqueous phase was extracted with ethyl acetate. The combined organic phases were dried over sodium sulphate and concentrated in vacuo to afford (RS)-2-amino-2-(3-chloro-phenyl)-ethanol (1.84 g, quant.) as a yellow viscous oil. MS (ISP): 174.2 ( [{37C1}M+H]+), 172.2 ([{35C1}M+H]+).
 

Historical Records

Technical Information

Categories