Home Cart Sign in  
Chemical Structure| 5162-03-8 Chemical Structure| 5162-03-8
Chemical Structure| 5162-03-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of (2-Chlorophenyl)(phenyl)methanone

CAS No. :5162-03-8
Formula : C13H9ClO
M.W : 216.66
SMILES Code : ClC1=C(C=CC=C1)C(=O)C1=CC=CC=C1
MDL No. :MFCD00000558
InChI Key :VMHYWKBKHMYRNF-UHFFFAOYSA-N
Pubchem ID :78838

Safety of (2-Chlorophenyl)(phenyl)methanone

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of (2-Chlorophenyl)(phenyl)methanone

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5162-03-8 ]

[ 5162-03-8 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 917-64-6 ]
  • [ 5162-03-8 ]
  • [ 24892-81-7 ]
  • 2
  • [ 288-16-4 ]
  • [ 5162-03-8 ]
  • [ 118173-48-1 ]
  • 3
  • [ 5162-03-8 ]
  • [ 1357011-76-7 ]
  • [ 530-48-3 ]
  • [ 24892-81-7 ]
  • 4
  • [ 5162-03-8 ]
  • [ 1427190-91-7 ]
  • [ 1427174-98-8 ]
  • 5
  • [ 5906-98-9 ]
  • [ 100-47-0 ]
  • [ 5162-03-8 ]
  • 6
  • [ 5162-03-8 ]
  • [ 1779-49-3 ]
  • [ 24892-81-7 ]
YieldReaction ConditionsOperation in experiment
General procedure: To a 100 mL round bottom flask equipped with a Teflon coated stir bar was added methyltriphenylphosphonium bromide (15 mmol, 1.5 equiv) and THF (40 mL). The reaction mixture was cooled to 0 C and stirred. Once cooled, KOtBu (15 mmol, 1.5 equiv) was added and the system was removed from the ice bath and let stir at room temperature for 0.5 h. Next, ketone (10 mmol, 1 equiv) was added to the system which was then purged with N2 and heated to 50 C for 3 h. Upon completion, the reaction was quenched with water (20 mL), extracted with ether (250 mL), and dried with sufficient MgSO4. The resulting extracts were concentrated in vacuo and purified via flash column chromatography.
  • 7
  • [ 24892-81-7 ]
  • [ 5162-03-8 ]
YieldReaction ConditionsOperation in experiment
90.9% With oxygen; at 110℃; for 8h;Sealed tube; Add 0.5mmol of <strong>[24892-81-7]1-chloro-2-(1-phenylvinyl)benzene</strong> and 1mL polyethylene glycol dimethyl ether (MW=250) into a test tube as a solvent, seal the test tube, perform oxygen replacement, and insert the refill The balloon with pure oxygen was placed at 110C for 8 hours and the yield was 90.9%.
 

Historical Records

Technical Information

Categories