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Chemical Structure| 10146-04-0 Chemical Structure| 10146-04-0

Structure of 10146-04-0

Chemical Structure| 10146-04-0

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Product Details of [ 10146-04-0 ]

CAS No. :10146-04-0
Formula : C17H15N3
M.W : 261.32
SMILES Code : NC1=CC=C2C=CC=CC2=C1/N=N/C3=CC=C(C)C=C3

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Application In Synthesis of [ 10146-04-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10146-04-0 ]

[ 10146-04-0 ] Synthesis Path-Downstream   1~1

  • 1
  • p-toluenediazonium hydrogen sulfate [ No CAS ]
  • [ 81-16-3 ]
  • [ 10146-04-0 ]
YieldReaction ConditionsOperation in experiment
80% With hydrogenchloride; sodium nitrite; In water; at 0℃; for 0.5h; General procedure: To an aromatic or heteroaromatic amine (10 mmol) dissolvedin aqueous hydrochloric acid (15mL, 50%), sodiumnitrite (0.84 g, 8 mmol) was added in small portions at0C. After 30min, urea (1 g) was added, and the resultingmixture was poured into an aqueous/methanolicsolution (1:1, 50mL) of 2-aminonaphthalene sulfonic acid(2.2 g, 10 mmol). The product precipitated was isolatedby suction, washed with water, and recrystallized frombutanol after drying.
 

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