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Chemical Structure| 1016233-16-1 Chemical Structure| 1016233-16-1

Structure of 1016233-16-1

Chemical Structure| 1016233-16-1

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Product Details of [ 1016233-16-1 ]

CAS No. :1016233-16-1
Formula : C10H19NO2S
M.W : 217.33
SMILES Code : O=C(N1CC(CSC)C1)OC(C)(C)C

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Application In Synthesis of [ 1016233-16-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1016233-16-1 ]

[ 1016233-16-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 253176-94-2 ]
  • [ 5188-07-8 ]
  • [ 1016233-16-1 ]
YieldReaction ConditionsOperation in experiment
100% In water; acetonitrile; at 60℃; for 18h; A mixture of tert-butyl 3-(iodomethyl)azetidine-l-carboxylate (5.05 g, 17 mmol, 1 equiv.) and NaSMe (3.56 g, 25.5 mmol, 1.50 equiv.) in MeCN (30 mL) and LEO (10 mL) was heated to 60 C for 18 h. After cooling down to rt, the mixture was concentrated, the residue was diluted with EA. The organic solution was washed with water, dried over NaaSCL. This solution was concentrated to afford the title compound (3.69 g, quant.) as a light-yellow oil.
 

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