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Chemical Structure| 1030829-49-2 Chemical Structure| 1030829-49-2

Structure of 1030829-49-2

Chemical Structure| 1030829-49-2

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Product Details of [ 1030829-49-2 ]

CAS No. :1030829-49-2
Formula : C14H14O2
M.W : 214.26
SMILES Code : OCCC1=CC=CC=C1OC2=CC=CC=C2
MDL No. :MFCD20257410

Safety of [ 1030829-49-2 ]

Application In Synthesis of [ 1030829-49-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1030829-49-2 ]

[ 1030829-49-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 108-86-1 ]
  • [ 7768-28-7 ]
  • [ 1030829-49-2 ]
YieldReaction ConditionsOperation in experiment
54% With 2-acetonylpyridine; caesium carbonate; copper(I) bromide; In dimethyl sulfoxide; at 80℃; Preparation 18a: 2-(2-phenoxyphenyl)ethanol[00180] A mixture of 2-(2-hydroxyethyl)phenol (lg, 7.2 mmol), bromobenzene (1.70 g, 10.8 mmol), l-pyridin-2-yl-propan-2-one (194 mg, 1.44 mmol), CuBr (103 mg, 0.72 mmol) and Cs2C03(4.73 g, 14.5 mmol) in DMSO (20 mL) was stirred overnight at 80 °C, H20 was added, extracted with EtOAc, purified by flash column chromatography on silica gel (PE/EA=1/1) to afford the title compound (850 mg, 54percent). [M+H] Calc'd for C14H14O2, 215; Found, 215.
 

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