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Chemical Structure| 1051374-19-6 Chemical Structure| 1051374-19-6

Structure of 1051374-19-6

Chemical Structure| 1051374-19-6

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Product Details of [ 1051374-19-6 ]

CAS No. :1051374-19-6
Formula : C23H19NO3S
M.W : 389.47
SMILES Code : O=C([C@@H](N1)CSC(C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4)OC1=O
MDL No. :MFCD31630312

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Application In Synthesis of [ 1051374-19-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1051374-19-6 ]

[ 1051374-19-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 32315-10-9 ]
  • [ 2799-07-7 ]
  • [ 1051374-19-6 ]
YieldReaction ConditionsOperation in experiment
85% With cyclohexene; In ethyl acetate; for 3h;Reflux; Triphosgene (0.312 g, 1.05 mmol) was added to a mixture of compound 2.5 (STLC) (0.181 g, 0.5 mmol) and cyclohexene (0.410 g, 5 mmol) in ethyl acetate (5 mL) at 0° C. as is illustrated in Scheme G. The reaction mixture was allowed to reflux for 3 h. The volatiles were removed in vacuo to obtain the crude residue as pale yellow solid. The crude material was dissolved in methylene chloride (20 mL), washed with water (35 mL), organic layer was dried over anhydrous sodium sulfate, and the solvents were evaporated under reduced pressure to provide the product as colorless solid (0.165 g, 85percent). IR (KBr, cm?1): 3250, 2956, 1779, 1634, 1212. 1H NMR (300 MHz, CDCl3) delta 7.43-7.39 (m, 5H), 7.32-7.19 (m, 10H), 5.79 (s, 1H), 3.53-3.49 (m 1H), 2.78-2.63 (m, 2H); 13C NMR (75 MHz, CDCl3) delta 167.76, 151.00, 143.69, 129.33, 128.29, 127.26, 67.76, 56.46, 33.24.
 

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