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CAS No. : | 106820-63-7 | MDL No. : | MFCD01570165 |
Formula : | C9H11NO6S2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | KUTKKTKUSGIBPZ-UHFFFAOYSA-N |
M.W : | 293.32 | Pubchem ID : | 717593 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H312-H319-H332 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
79% | With sodium methylate In methanol for 2 h; Reflux | 8.5 g of TNXK-1, 27percent sodium methoxide 27.2 g and anhydrous methanol 15 ml stirring to reflux 2 hours, cooling, water 200 ml dilution, use 10percent hydrochloric acid to neutral, evaporate the solvent, and then cooling the residue 10percent hydrochloric acid to the PH is 3. Filtering, the filter cake is then washing with water, drying, be 5.6 g yellow-green solid TNXK-2, yield 79percent. |
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