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[ CAS No. 108343-90-4 ]

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2D
Chemical Structure| 108343-90-4
Chemical Structure| 108343-90-4
Structure of 108343-90-4 *Storage: {[proInfo.prStorage]}

Quality Control of [ 108343-90-4 ]

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Related Doc. of [ 108343-90-4 ]

SDS

Product Details of [ 108343-90-4 ]

CAS No. :108343-90-4MDL No. :MFCD08752814
Formula :C9H13NO2Boiling Point :-
Linear Structure Formula :-InChI Key :N/A
M.W :167.21Pubchem ID :10352062
Synonyms :

Computed Properties of [ 108343-90-4 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 108343-90-4 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P305 P351 P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 108343-90-4 ]

  • Downstream synthetic route of [ 108343-90-4 ]

[ 108343-90-4 ] Synthesis Path-Downstream   1~10

  • 1
  • [ 108343-90-4 ]
  • C40H44F5N3O8 [ No CAS ]
  • 2
  • [ 108343-90-4 ]
  • C33H38BrF4N3O7 [ No CAS ]
  • 3
  • [ 108343-90-4 ]
  • [ 869984-48-5 ]
  • 4
  • [ 108343-90-4 ]
  • [ 869984-51-0 ]
  • 5
  • [ 108343-90-4 ]
  • [ 869984-25-8 ]
  • 6
  • [ 108343-90-4 ]
  • C21H18BrF4N3O3 [ No CAS ]
  • 7
  • [ 108343-90-4 ]
  • C38H40F5N3O8 [ No CAS ]
  • 8
  • [ 108343-90-4 ]
  • 5-(2-{1-amino-2-[5-(2-fluoro-3-methoxy-phenyl)-3-(2-fluoro-6-trifluoromethyl-benzyl)-4-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl]-ethyl}-phenoxy)-pentanoic acid [ No CAS ]
  • 9
  • [ 62717-78-6 ]
  • [ 108343-90-4 ]
  • 10
  • 2-(benzylamino)-2-(2-methoxyphenyl)ethanol [ No CAS ]
  • [ 108343-90-4 ]
YieldReaction ConditionsOperation in experiment
95% With 10 wt% Pd(OH)2 on carbon; ammonium formate; In methanol; at 70℃; for 2.5h; In a 250-ml triple-neck flask, 7 g (27.2 mmol) of 2-(benzylamino)-2-(2-methoxyphenyl)ethanol obtained previously are solubilized in 100 ml of methanol. 0.7 g of Pd(OH)2/C and 8.6 g (136 mmol) of ammonium formiate are added, and then the medium is brought to 70 C. for 2.5 h. After return to room temperature, the palladium is filtered on Celite, rinsed with 20 methanol and the filtrate is concentrated and purified by flash chromatography on silica gel (eluent: dichloromethane/methanol/NH4OH=90/9/1%). 4.3 g (25.7 mmol) of [108343-90-4]2-amino-2-(2-methoxyphenyl)ethanol are recovered in the form of a clear oil. Yield: 95%. 1H NMR (CDCl3) delta: 2.02 (ls, 3H); 3.61 (m, 1H); 3.74 (dd, 1H, J=10.3 and 2.4 Hz); 3.84 (s, 3H); 4.26 (m, 1H); 6.88 (m, 1H); 6.95 (m, 1H); 7.26 (m, 2H).
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