Home Cart Sign in  
Chemical Structure| 1103929-71-0 Chemical Structure| 1103929-71-0

Structure of 1103929-71-0

Chemical Structure| 1103929-71-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1103929-71-0 ]

CAS No. :1103929-71-0
Formula : C12H12ClNO6
M.W : 301.68
SMILES Code : O=C(O)COCC(NC1=CC=C(Cl)C=C1C(OC)=O)=O
MDL No. :MFCD27964573

Safety of [ 1103929-71-0 ]

Application In Synthesis of [ 1103929-71-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1103929-71-0 ]

[ 1103929-71-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1103929-71-0 ]
  • [ 157837-31-5 ]
  • [ 1190223-05-2 ]
YieldReaction ConditionsOperation in experiment
65% General procedure: A mixture of the carboxylic acid (6a) (1 g, 3.31 mmol), DMF (cat. amount), oxalyl chloride (3.98mmol) in THF (20 mL) was stirred at 0C for 30 min. After the mixture was concentrated to dryness invacuo, a solution of the amine (8g) (3.64 mmol) in DMA (10 mL) was added at 0C thereto. The mixturewas stirred overnight at room temperature, diluted with an aqueous NaHCO3 solution and extracted withAcOEt. The organic layer was separated, washed with water, dried over Na2SO4. After the solvent wasdistilled off under reduced pressure, the resulting crude product was purified by silica gel columnchromatography to afford the corresponding amide (12g) as a solid (1.34 g, 79%).
  • 2
  • [ 1103929-71-0 ]
  • [ 157837-31-5 ]
  • [ 1190221-55-6 ]
 

Historical Records