Alternatived Products of [ 113075-74-4 ]
Product Details of [ 113075-74-4 ]
CAS No. : | 113075-74-4 |
MDL No. : | MFCD16037864 |
Formula : |
C10H11ClO
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
182.65
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 113075-74-4 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 113075-74-4 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 113075-74-4 ]
- 1
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[ 26673-30-3 ]
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[ 113075-74-4 ]
Yield | Reaction Conditions | Operation in experiment |
|
With hydrogenchloride; sodium borohydrid; |
(a) 20.6 g of <strong>[26673-30-3]5-chloro-1-tetralone</strong> were dissolved in 100 ml of alcohol, whereupon 2.2 g of sodium borohydride were added portionwise. The reaction mixture was stirred at 40 for 2 hours, then cooled and thereupon treated at room temperature with 32 ml of 2N hydrochloric acid. The mixture was then concentrated in vacuo and extracted with methylene chloride. The organic phases were dried over sodium sulphate and evaporated. The 5-chloro-1-tetralol which remains behind as the residue was processed directly as the crude product. |
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