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Chemical Structure| 113206-07-8 Chemical Structure| 113206-07-8

Structure of 113206-07-8

Chemical Structure| 113206-07-8

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Product Details of [ 113206-07-8 ]

CAS No. :113206-07-8
Formula : C8H5Cl2NOS
M.W : 234.10
SMILES Code : COC1=CC=C(SC(Cl)=N2)C2=C1Cl
MDL No. :N/A

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Application In Synthesis of [ 113206-07-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 113206-07-8 ]

[ 113206-07-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 55690-60-3 ]
  • [ 113206-07-8 ]
YieldReaction ConditionsOperation in experiment
With sulfuryl dichloride; at 0 - 20℃; for 2h; Sulfuryl chloride (10 mL) was added to 5-methoxy-2- mercaptobenzothiazole at 0 0C. After complete addition, the reaction mixture was allowed to warm to it. After 2 h, the reaction mixture was poured into ice water (100 mL). This was allowed to warm to rt and was extracted with EtOAc (3 x). The combined organics were dried over Na2SO4, filtered, and concentrated under reduced pressure. The material was used without further purification. LC-MS: RT = 9.08 min., [M+H]+ = 234.0.
 

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