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CAS No. : | 1147558-43-7 | MDL No. : | MFCD18426013 |
Formula : | C7H4ClFN2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 170.57 g/mol | Pubchem ID : | 68039995 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302 | Packing Group: | |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
88% | With N-chloro-succinimide In acetonitrile at 85℃; for 5 h; | 4-Amino-3-chloro-5-fluorobenzonitrile A mixture of 4-amino-3-fluorobenzonitrile (1 equiv.) and N-chlorosuccinimide (1.5 equiv.) in acetonitrile (0.24 M) was stirred at 85° C. for 5 h. The solvent was removed by concentration and the residue was partitioned between ethyl acetate and 5percent NaOH. The organic phase was washed with 5percent NaOH and brine. Then the organic phase was dried over MgSO4 and dried in vacuum to afford 4-amino-3-chloro-5-fluorobenzonitrile (88percent) as a beige solid. 1H NMR (400 MHz, CDCl3) δ ppm: 7.41 (t, J=6 Hz, 1H), 7.24 (dd, J=1.8, 10.2 Hz, 1H), 4.66 (s, 2H). |
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