Home Cart Sign in  
Chemical Structure| 115054-62-1 Chemical Structure| 115054-62-1

Structure of 115054-62-1

Chemical Structure| 115054-62-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 115054-62-1 ]

CAS No. :115054-62-1
Formula : C11H16ClNO4
M.W : 261.70
SMILES Code : O=C(OC)[C@@](C)(N)CC1=CC=C(O)C(O)=C1.[H]Cl

Safety of [ 115054-62-1 ]

Application In Synthesis of [ 115054-62-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 115054-62-1 ]

[ 115054-62-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 555-30-6 ]
  • [ 115054-62-1 ]
YieldReaction ConditionsOperation in experiment
97% With thionyl chloride; at -15 - 20℃; for 72.0h;Heating / reflux; A suspension of 29.7 g (141 mmol) of alpha-methyl-L-DOPA in 300 mL of absolute methanol was cooled to -15 C. and treated with 125.8 g (1.06 mol) thionyl chloride under a nitrogen atmosphere. The reaction was allowed to warm to ambient temperature and stir at reflux for 3 days. Concentration followed by trituration with ether gave 31.7 g (97%) as an off-white solid: NMR (DMSO-d6) delta1.47 (s, 3H), 2.92 (d, J=12 Hz, 1H), 2.98 (d, J=12 Hz, 1H), 3.74 (s, 3H), 6.41 (d of d, J=9 Hz AND 2 Hz, 1H), 6.54 (d, J=2 Hz, 1H), 6.68 (d, J=9 Hz, 1H), 8.46-8.90 (br s, 3H), 8.93 (s, 1H), 8.96 (s, 1H).
 

Historical Records