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Chemical Structure| 1152237-10-9 Chemical Structure| 1152237-10-9

Structure of 1152237-10-9

Chemical Structure| 1152237-10-9

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Product Details of [ 1152237-10-9 ]

CAS No. :1152237-10-9
Formula : C14H9BrN2O
M.W : 301.14
SMILES Code : O=C1NC(C2=CC=CC=C2)=NC3=C1C=CC(Br)=C3
MDL No. :MFCD30290930

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Application In Synthesis of [ 1152237-10-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1152237-10-9 ]

[ 1152237-10-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 100-52-7 ]
  • [ 112253-70-0 ]
  • [ 1152237-10-9 ]
YieldReaction ConditionsOperation in experiment
69% With sodium metabisulfite; In ISOPROPYLAMIDE; for 3h;Reflux; Synthesis of 4:A mixture of 3 (1.5 g, 7.2 mmol) with benzaldehyde (0.73 mL, 7.2 mmol) and sodium bisulfite (1.1 g, 10.8 mmol) in dimethylacetamide (DMA) (5 mL) was heated at reflux for 3 h. After pouring into H2O (20 mL), the solution was allowed to warm up to room temperature. The solid which formed was filtered, washed with H2O, followed by Et2O to provide 4 (1.5 g, 69%) as a yellow solid, after recrystallization with MeOH/EtOAc.
 

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