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Chemical Structure| 115363-11-6 Chemical Structure| 115363-11-6

Structure of 115363-11-6

Chemical Structure| 115363-11-6

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Product Details of [ 115363-11-6 ]

CAS No. :115363-11-6
Formula : C14H12O2
M.W : 212.24
SMILES Code : O=C(C1=C(C)C(C2=CC=CC=C2)=CC=C1)O
MDL No. :MFCD11554177

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Application In Synthesis of [ 115363-11-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 115363-11-6 ]

[ 115363-11-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 76350-90-8 ]
  • [ 115363-11-6 ]
YieldReaction ConditionsOperation in experiment
28 g With Jones reagent; In acetone; at 25℃; for 6h; Pour 40 g of CrO3 into a volumetric flask containing 120 mL of water, add 34.5 mL of concentrated H2SO4, shake well, and dilute to 150 mL with water to obtain Jones reagent.30 g of <strong>[76350-90-8]2-methyl-3-phenylbenzyl alcohol</strong> were added to the three-necked flask,32mL water, 200mL acetone, ice water bath, drop 90mL Jones reagent, control reaction temperature is 25 C, reaction 6 h,The reaction was followed by thin layer chromatography, and dichloromethane was used as a developing solvent. After the substrate point disappeared and the aldehyde point disappeared, the reaction was stopped, and the reaction took 6 h.The acetone was removed under reduced pressure, a large amount of precipitate was produced, suction filtration, and the filter cake was washed with water to whiteness, and dried to obtain a crude product of 30 g yield 99%.The crude product was dissolved in ethanol (the amount of ethanol was twice the mass of the product) and heated at 60 C.All were dissolved, filtered, and the filtrate was cooled to -10 C under electric stirring, and then the crystals were suction filtered, dried to obtain 28 g, and the melting point was measured at a melting point of 151-153 C.
 

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