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Chemical Structure| 116296-36-7 Chemical Structure| 116296-36-7

Structure of 116296-36-7

Chemical Structure| 116296-36-7

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Product Details of [ 116296-36-7 ]

CAS No. :116296-36-7
Formula : C10H14N2O
M.W : 178.23
SMILES Code : CC(NC1=C(C)C=C(N)C=C1C)=O
MDL No. :MFCD09966010

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Application In Synthesis of [ 116296-36-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 116296-36-7 ]

[ 116296-36-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 116296-36-7 ]
  • [ 16947-63-0 ]
YieldReaction ConditionsOperation in experiment
97% 2,6-Dimethyl-4-nitro-phenylamine.; Concentrated hydrochloric acid (17.5 rnL) was added to iV-(2,6-dimethyl-4-nitro-phenyl)- acetamide (5.05 g) and heated to 140 0C for 30 minutes in a sealed microwave process vial. The reaction mixture was neutralized with solid sodium carbonate in water and the precipitated product was collected by filtration and washed with water (100 mL) to furnish 3.93 g (97% yield) of the title compound as a yellow solid. 1H NMR (500 MHz, DMSOd6): 2.15 (s, 6H), 6.15 (b, 2H), 7.79 (s, 2H).
 

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